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Nanocrystalline Fe/Zr alloys: preparation by using mechanical alloying and mechanical milling processes

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Abstract

Nanocrystalline Fe/Zr alloys have been prepared after milling for 9 h the mixture of elemental Fe and Zr powders or the arc-melting produced Fe2Zr alloy by using mechanical alloying and mechanical milling techniques, respectively. X-ray and Mössbauer results of the Fe and Zr powders, mechanically alloyed, suggest that amorphous Fe2Zr phase and \(\upalpha\)-Fe(Zr) nanograins have been produced with relative concentrations of 91% and 9%, respectively. Conversely, the results of the mechanically milled Fe2Zr alloy indicate that nanograins of the Fe2Zr alloy have been formed, surrounded by a magnetic inter-granular phase that are simultaneously dispersed in a paramagnetic amorphous phase.

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Authors and Affiliations

  1. Facultad de Ciencias Físicas, Universidad Nacional Mayor de San Marcos, P.O. Box 14-149, Lima, 14, Peru

    V. A. Peña Rodríguez, J. Medina Medina, J. Quispe Marcatoma, Ch. Rojas Ayala & C. V. Landauro

  2. Centro Brasileiro de Pesquisas Físicas, Rua. Dr. Xavier Sigaud 150, Urca, CEP 22290-180, Rio de Janeiro, Brazil

    E. M. Baggio-Saitovitch

  3. Depto. de Física, Universidade Federal do Espírito Santo, CEP 29075-910, Vitória, Espírito Santo, Brazil

    E. C. Passamani

Authors
  1. V. A. Peña Rodríguez
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  2. J. Medina Medina
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  3. J. Quispe Marcatoma
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  4. Ch. Rojas Ayala
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  5. C. V. Landauro
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  6. E. M. Baggio-Saitovitch
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  7. E. C. Passamani
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Correspondence to V. A. Peña Rodríguez.

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Rodríguez, V.A.P., Medina, J.M., Marcatoma, J.Q. et al. Nanocrystalline Fe/Zr alloys: preparation by using mechanical alloying and mechanical milling processes. Hyperfine Interact 202, 145–151 (2011). https://doi.org/10.1007/s10751-011-0343-3

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  • DOI: https://doi.org/10.1007/s10751-011-0343-3

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