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Magnetic Properties and Crystallization of the Fe75Si15B10 Amorphous Alloy Prepared by Mechanical Alloying

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Abstract

The magnetic order and crystallization of the amorphous Fe75Si15B10 alloy prepared by mechanical alloying was studied in situ by 57Fe Mössbauer spectroscopy. These measurements were carried out using a vacuum furnace, controlling the temperature in the absorber. From Mössbauer measurements the magnetic order temperature of the as-milled sample was estimated at about 675 K. In order to identify the crystalline phases formed during heating, Mössbauer measurements were analyzed together with X-ray diffraction analysis. Both results show the formation of several crystalline phases such as Fe5SiB2, Fe2B, Fe3Si, α-Fe, Fe–B composite and a residual amorphous phase.

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Authors and Affiliations

  1. Facultad de Ciencias Físicas, Universidad Nacional Mayor de San Marcos, P.O. Box 14-0149, Lima 14, Perú

    J. Quispe Marcatoma & V. A. Peña Rodríguez

  2. Centro Brasileiro de Pesquisas Físicas, Rua Dr. Xavier Sigaud 150, Urca, CEP, 22290-180, Rio de Janeiro, Brazil

    E. M. Baggio-Saitovitch

Authors
  1. J. Quispe Marcatoma
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  2. V. A. Peña Rodríguez
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  3. E. M. Baggio-Saitovitch
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Quispe Marcatoma, J., Peña Rodríguez, V.A. & Baggio-Saitovitch, E.M. Magnetic Properties and Crystallization of the Fe75Si15B10 Amorphous Alloy Prepared by Mechanical Alloying. Hyperfine Interactions 148, 97–102 (2003). https://doi.org/10.1023/B:HYPE.0000003769.28718.19

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  • DOI: https://doi.org/10.1023/B:HYPE.0000003769.28718.19

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