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Insecticide residues in California citrus fruits and products

  • Conference paper
Residue Reviews / Rückstands-Berichte

Part of the book series: Reviews of Environmental Contamination and Toxicology ((RECT,volume 28))

Abstract

Prior to about 1945 it was not realized that spray and dust deposits of most organic insecticidal1 chemicals penetrated, in the field, into subsurface regions of sprayed citrus fruits, even though they were generally nonsystemic in action, as with some of the DN compounds and rotenone. Also, emphasis on “residues” (deposits) prior to this same time was on correlations with pest-control efficacy rather than on safe consumption of the treated commodity, so that initial deposits and aged deposits were most often obtained as weight of insecticide per unit areas of leaf (foliage) tissue2 rather than on and in mature fruits, as with sulfur, lime-sulfur, and lead arsenate, because insect populations were usually evaluated on leaves or twigs rather than on fruits. In connection with the field performance of DDT and other new insecticides against insects and mites in citriculture, however, it was realized shortly after 1940 that the slow disappearance or attenuation from leaves of these (DDT) surface deposits and effective residues from organic pesticides signified at least partial penetration into subsurface tissues (Gunther 1946 and Gunther et al. 1946).

Presented in partial and summary form at the International Citrus Symposium, 19 March 1968, Riverside, California: see Gunther and Westlake (1968) in “References” section.

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References

  • Anderson, C. A., D. MacDougall, J. W. Kesterson, R. Hendrickson, and R. F. Brooks: Effects of processing on Guthion residues in oranges and orange products. J. Agr. Food Chem. 11, 422 (1963).

    Article  CAS  Google Scholar 

  • Anonymous: Reduced tolerance for DDT. Federal Register, Feb. 19 (1968 a).

    Google Scholar 

  • Anonymous: Italian pesticide regulation for fruits and vegetables. Gazzetta Ufficiale della Repubblica Italiana, No. 28, pp. 634–639, Feb. 1 (1968 b).

    Google Scholar 

  • Atkins, E. L., R. C. Blinn, T. R. Fukuto, and F. A. Gunther: Residues on oranges resulting from the use of DDT, parathion, Phosdrin, and TDE for the control of orangeworms. J. Econ. Entomol. 54, 455 (1961).

    Google Scholar 

  • Balson, E. W.: Vapor-pressure measurement. III. An effusion manometer sensitive to 5 × 10-6 millimeters of mercury: Vapor pressures of DDT and other slightly volatile substances. Trans. Faraday Soc. 43, 48 (1947).

    Article  CAS  Google Scholar 

  • Barnes, M. M., G. E. Carman, W. H. Ewart, and F. A. Gunther: Fruit surface residues of DDT and parathion at harvest. Adv. Chem. Series 1, 112 (1950).

    Google Scholar 

  • Benyon, K. I., and K. E. Elgar: The analysis for residues of chlorinated insecticides and acaricides. Analyst 91, 143 (1966).

    Article  Google Scholar 

  • Blinn, R. C., G. E. Carman, W. H. Ewart, and F. A. Gunther: Residual behavior of various insecticides on and in lemons and oranges. J. Econ. Entomol. 52, 42 (1959 a).

    CAS  Google Scholar 

  • Blinn, R. C., R. W. Dorner, J. H. Barkley, L. R. Jeppson, F. A. Gunther, and C. C. Cassil: Locale of aged Tedion residues on citrus fruits. J. Econ. Entomol. 52, 723 (1959 b).

    CAS  Google Scholar 

  • Blinn, R. C., R. W. Dorner, F. A. Gunther, and M. J. Kolbezen: Microdetermination of the acaricide ethyl p,p′-dichlorobenzilate (Chlorobenzilate). J. Agr. Food Chem. 2, 1080 (1954).

    Article  CAS  Google Scholar 

  • Boyce, A. M.: Personal communication (1946).

    Google Scholar 

  • Bright, N. F. H., J. C. Cuthill, and N. H. Woodbury: Vapor pressure of parathion and related compounds. J. Sci. Food Agr. 1, 344 (1950).

    Article  CAS  Google Scholar 

  • Burke, J. A.: Report on chlorinated insecticides and miticides. J. Assoc. Official Anal. Chemists 50, 575 (1967).

    Google Scholar 

  • Carman, G. E., W. H. Ewart, M. M. Barnes, and F. A. Gunther: Absorption of DDT and parathion by fruits. Adv. Chem. Series 1, 128 (1950).

    Google Scholar 

  • Carman, G. E., F. A. Gunther, R. C. Blinn, and R. D. Garmus: The physical fate of parathion applied to citrus. J. Econ. Entomol. 45, 767 (1952).

    CAS  Google Scholar 

  • Cook, J. W.: Persistence of residues in foods. In C. O. Chichester (ed.): Research in pesticides, pp. 205–212. New York: Academic Press (1965).

    Google Scholar 

  • Crafts, A. S., and C. L. Foy: The chemical and physical nature of plant surfaces in relation to the use of pesticides and to their residues. Residue Reviews 1, 112 (1962).

    CAS  Google Scholar 

  • de Vos, R. H.: Sampling and analysis for biphenyl residues in citrus fruit. Proc. Internat. Citrus Symposium, Riverside, Calif., Mar. 16–26 (1968). In press.

    Google Scholar 

  • Division of Agricultural Sciences of the University of California: 1968/1969 Treatment guide for California citrus crops. California Agricultural Experiment Station Extension Service, Berkeley, Calif. (1968/1969).

    Google Scholar 

  • Ebeling, W.: Analysis of the basic processes involved in the deposition, degradation, persistence, and effectiveness of pesticides. Residue Reviews 3, 35 (1963).

    CAS  Google Scholar 

  • Ewart, W. H., H. S. Elmer, and F. A. Gunther: Parathion treatments for the control of citricola scale on citrus in California. J. Econ. Entomol. 44, 598 (1951).

    CAS  Google Scholar 

  • Fahey, J. E.: Digest of the literature, 1925 through 1952, relating to sampling of crops for spray residue analyses. U. S. Department of Agriculture Mimeo., 59 pp. (1953).

    Google Scholar 

  • Forcier, G. A., and J. W. Olver: Simplified purification of acetonitrile for electroanalytical applications. Anal. Chem. 37, 1447 (1965).

    Article  Google Scholar 

  • Frear, D. E. H.: Pesticide residue investigations on raw agricultural commodities. Pennsylvania State University Agr. Expt. Station Bull. 703 (1963).

    Google Scholar 

  • Garber, M. J.: Statistical evaluation of results and sampling procedures. In G. Zweig (ed.): Analytical methods for pesticides, plant growth regulators, and food additives, Vol. 1, pp. 491–530. New York: Academic Press (1963).

    Google Scholar 

  • Gaston, L. K., J. H. Barkely, D. E. Ott, F. E. Hearth, L. R. Jeppson, and F. A. Gunther: Persistence of Morestan residues on and in citrus fruits by five complementary analytical methods. J. Agr. Food Chem., in press (1969).

    Google Scholar 

  • Gunther, F. A.: Aspects of the chemistry of DDT. J. Chem. Ed. 22, 238 and 279 (1945).

    Article  CAS  Google Scholar 

  • Gunther, F. A.: Chemical studies of DDT as an insecticide. 30th Ann. Meeting, Pacific Slope Branch Amer. Assoc. Econ. Entomol., Riverside, Calif., June 26–28 (1946).

    Google Scholar 

  • Gunther, F. A.: Unpublished data (1950).

    Google Scholar 

  • Gunther, F. A.: Instrumentation in pesticide residue determinations. Adv. Pest Control Research 5, 191 (1962).

    CAS  Google Scholar 

  • Gunther, F. A.: Advances in analytical detection of pesticides. In: Scientific aspects of pest control, pp. 276–302. Nat. Acad. Sci.-Nat. Research Council, Washington, D.C., Publ. No. 1402 (1966).

    Google Scholar 

  • Gunther, F. A.: Current status of pesticide residue methodology. In: Biological effects of pesticides in mammalian systems. N.Y. Acad. Sci., New York City, in press (1968 a).

    Google Scholar 

  • Gunther, F. A.: Unpublished data (1968 b).

    Google Scholar 

  • Gunther, F. A., and R. C. Blinn: Analysis of insecticides and acaricides. New York: Interscience (1955).

    Google Scholar 

  • Gunther, F. A., and R. C. Blinn: Persistng insecticide residues in plant materials. Ann. Review Entomol. 1, 167 (1956).

    Article  CAS  Google Scholar 

  • Gunther, F. A., and R. C. Blinn: Ultraviolet spectrophotometric microdetermination of the acaricide 4,4′-dichloro-alpha-(trichloromethyl)-benzhydrol (FW-293). J. Agr. Food Chem. 5, 517 (1957 a).

    Article  CAS  Google Scholar 

  • Gunther, F. A., and F. Buzzetti: Occurrence, isolation, and identification of polynuclear hydrocarbons as residues. Residue Reviews 9, 90 (1965).

    PubMed  CAS  Google Scholar 

  • Gunther, F. A., and L. R. Jeppson: Ovotran residues in citrus. University of California Citrus Expt. Sta. Mimeo., 20 pp., Nov. 15 (1951).

    Google Scholar 

  • Gunther, F. A., and L. R. Jeppson: Residues of p-chlorophenyl-p-chlorobenzenesulfonate (Compound K-6451) on and in lemons and oranges. J. Econ. Entomol. 47, 1027 (1954).

    CAS  Google Scholar 

  • Gunther, F. A., and W. E. Westlake: Studies of organic insecticide residues in California citrus fruits and products. Proc. Internat. Citrus Symposium, Riverside, Calif., Mar. 16–26 (1968). In press.

    Google Scholar 

  • Gunther, F. A., and M. M. Barnes, and G. E. Carman: Removal of DDT and parathion residues from apples, pears, lemons, and oranges. Adv. Chem. Ser. 1, 137 (1950).

    Article  Google Scholar 

  • Gunther, F. A., J. H. Barkley, and W. H. Ewart: Harvest residues of apparent dieldrin in peel and juice of navel oranges. J. Econ. Entomol. 47, 1033 (1954).

    CAS  Google Scholar 

  • Gunther, F. A., R. C. Blinn, and J. H. Barkley: Infrared procedure for quantitative determination of residues of 2,4,4′,5-tetrachlorodiphenyl sulfone (Tedion) on and in citrus fruit peel. J. Agr. Food Chem. 7, 104 (1959 a).

    Article  CAS  Google Scholar 

  • Gunther, F. A., R. C. Blinn, and G. E. Carman: Residues of Sevin on and in lemons and oranges. J. Agr. Food Chem. 10, 222 (1962 a).

    Article  CAS  Google Scholar 

  • Gunther, F. A., R. C. Blinn, and G. E. Carman: Residues of ethion on and in lemons and oranges as determined by an infrared spectrophotometric procedure. J. Agr. Food Chem. 10, 224 (1962 b).

    Article  Google Scholar 

  • Gunther, F. A., R. C. Blinn, L. R. Jeppson, J. H. Barkley, G. J. Frisone, and R. D. Garmus: Field persistence of the acaricide 4,4′-dichloro-alpha-(trichloromethyl)-benz-hydrol (FW-293) on and in mature lemons and oranges. J. Agr. Food Chem. 5, 595 (1957 b).

    Article  CAS  Google Scholar 

  • Gunther, F. A., R. C. Blinn, M. J. Kolbezen, J. H. Barkley, W. D. Harris, and H. S. Simon: Microestimation of 2-(p-tert-butylphenoxy)isopropyl-2-chloroethyl sulfite residues. Anal. Chem. 23, 1835 (1951).

    Article  CAS  Google Scholar 

  • Gunther, F. A., F. Buzzetti, and W. E. Westlake: Residue behavior of polynuclear hydrocarbons on and in oranges. Residue Reviews 17, 81 (1967).

    PubMed  CAS  Google Scholar 

  • Gunther, F. A., G. E. Carman, R. C. Blinn, and J. H. Barkley: Persistence of residues of Guthion on and in mature lemons and oranges and in laboratory-processed citrus “pulp” cattle feed. J. Agr. Food Chem. 11, 424 (1963).

    Article  CAS  Google Scholar 

  • Gunther, F. A., G. E. Carman, L. R. Jeppson, J. H. Barkley, R. C. Blinn, and G. G. Patchett: Residual behavior of S-(p-chlorophenylthio) methyl O,O-diethyl phosphoro-dithioate (Trithion) on and in mature lemons and oranges, J. Agr. Food Chem. 7, 28 (1959 b).

    Article  CAS  Google Scholar 

  • Gunther, F. A., W. H. Ewart, J. H. Barkley, and R. T. Murphy: Persistence of residues of dimethoate on and in mature Valencia oranges and in laboratory-processed citrus pulp cattle feed. J. Agr. Food Chem. 13, 548 (1965).

    Article  CAS  Google Scholar 

  • Gunther, F. A., W. H. Ewart, R. C. Blinn, H. S. Elmer, and G. B. Wacker: Field persistence comparisons of residues of the insecticide, Diazinon, in lemons and Valencia oranges and effects on juice flavor. J. Agr. Food Chem. 6, 521 (1958 a).

    Article  CAS  Google Scholar 

  • Gunther, F. A., J. W. Hylin, and R. E. Spenger: Nature of chlorine interferences in total halogen methods of analysis of organochlorine pesticide residues in plants. J. Agr. Food Chem. 14, 515 (1966).

    Article  CAS  Google Scholar 

  • Gunther, F. A., L. R. Jeppson, J. H. Barkley, L. M. Elliott, R. C. Blinn, and C. L. Dunn: Persistence of residues of 2,3-p-dioxanedithiol S,S-bis(O,O-diethyl phosphorodithioate) as an acaricide on and in mature lemons and oranges. J. Agr. Food Chem. 6, 210 (1958 b).

    Article  CAS  Google Scholar 

  • Gunther, F. A., L. R. Jeppson, and G. B. Wacker: Persistence of chlorobenzilate residues in mature lemon fruits. J. Econ. Entomol. 48, 372 (1955).

    CAS  Google Scholar 

  • Gunther, F. A., D. L. Lindgren, M. I. Elliot, and J. P. La Due: Persistence of certain DDT deposits under field conditions. J. Econ. Entomol. 39, 624 (1946).

    PubMed  CAS  Google Scholar 

  • Gunther, F. A., W. E. Westlake, and P. S. Jaglan: Reported solubilities of 738 pesticide chemicals in water. Residue Reviews 20, 1 (1968).

    PubMed  CAS  Google Scholar 

  • Harden, L. J., and C. T. Sarten: Comparison of five extraction procedures for the recovery of DDT residues in field-treated collards. J. Assoc. Official Agr. Chemists 45, 988 (1962).

    Google Scholar 

  • Harris, T. H., and J. G. Cummings: Enforcement of the Federal Insecticide, Fungicide, and Rodenticide Act in the United States. Residue Reviews 6, 104 (1964).

    Google Scholar 

  • Hazleton Laboratories, Inc.: Final report: Market research project for 1966–1967. Dec. 8 (1967).

    Google Scholar 

  • Hazleton Laboratories, Inc.: Progress report French residue project. Mar. 13 (1968).

    Google Scholar 

  • Hazleton, L. W.: Sampling and analysis for various pesticides in single samples of citrus fruits. Proc. Internat. Citrus Symposium, Riverside, Calif., Mar. 16–26 (1968). In press.

    Google Scholar 

  • Hearth, F. E., D. E. Ott, and F. A. Gunther: Oscillopolarographic analysis of Morestan residues in Valencia orange rind following thin-layer chromatography. J. Assoc. Official Anal. Chemists 49, 774 (1966).

    CAS  Google Scholar 

  • Hindin, E.: Residue analyses in water resources. In G. Zweig (ed.): Analytical methods for pesticides, plant growth regulators, and food additives, vol. V, p. 90. New York: Academic Press (1967).

    Google Scholar 

  • Hoskins, W. M.: Methods for expressing the persistence of insecticidal residues on plants. Final report, Calif. contributing project to U.S. Department of Agriculture regional project W-45 (1961).

    Google Scholar 

  • Hull, H. M.: A tabular summary of research dealing with translocation of foliar-applied herbicides and selected growth regulators. Weeds 8, 214 (1960).

    Article  CAS  Google Scholar 

  • IsHii, A.: Personal communication (Mar. 30, 1968).

    Google Scholar 

  • Jasinski, R. J., and S. Kirkland: Analysis and distillation of propylene carbonate. Anal. Chem. 39, 1663 (1967).

    Article  CAS  Google Scholar 

  • Jeppson, L. R., L. M. Elliott, and F. A. Gunther: Persistence of residues of Neotran on and in mature lemons and oranges. J. Econ. Entomol. 51, 914 (1958).

    CAS  Google Scholar 

  • Jeppson, L. R., F. A. Gunther, and J. H. Barkley. Manuscript in preparation (1968).

    Google Scholar 

  • Klein, A. K.: Report on extraction procedures for chloro-organic pesticides. J. Assoc. Official Agr. Chemists 41, 551 (1958).

    CAS  Google Scholar 

  • Klein, A. K.: Determination of DDT in leafy vegetables. J. Assoc. Official Agr. Chemists 43, 703 (1960).

    CAS  Google Scholar 

  • Klein, A. K., E. P. Laug, and J. D. Sheehan, Jr.: Extraction procedures for chloro-organic insecticides. J. Assoc. Official Agr. Chemists 42, 539 (1959).

    CAS  Google Scholar 

  • Linskens, H. F., W. Heinen, and A. L. Stoffers: Cutícula of leaves and the residue problem. Residue Reviews 8, 136 (1965).

    CAS  Google Scholar 

  • Lykken, L.: Important considerations in collecting and preparing crop samples for residue analysis. Residue Reviews 3, 19 (1963).

    CAS  Google Scholar 

  • Melnikov, N. N.: Personal communication (Aug. 8, 1968).

    Google Scholar 

  • Menzie, C. M.: Metabolism of pesticides. U.S. Department of Interior, Fish and Wildlife Service, Bureau of Sport Fisheries and Wildlife, Washington, D.C., Special Sci. Rep’t. Wildlife No. 96, May (1966).

    Google Scholar 

  • Mestres, R.: Pesticides in citrus fruits on the French market. Proc. Internat. Citrus Symposium, Riverside, Calif., Mar. 16–26 (1968). In press.

    Google Scholar 

  • Metcalf, R. L., and R. B. March: Behavior of octamethyl pyrophosphoramide in in citrus plants. J. Econ. Entomol. 45, 988 (1952).

    CAS  Google Scholar 

  • Metcalf, R. L., T. R. Fukuto, and R. B. March: Plant metabolism of Dithio-Systox and Thimet. J. Econ. Entomol. 50, 338 (1957).

    CAS  Google Scholar 

  • Metcalf, R. L., R. B. March, and T. R. Fukuto: Study of systemic insecticides: Location and amount of residue in plant tissues determined with aid of radio-phosphorus tracers. Calif. Agr. 8(6), 5 (1954 a).

    Google Scholar 

  • Metcalf, R. L., R. B. March, and T. R. Fukuto, and M. G. Maxon: The behavior of Systox isomers in bean and citrus plants. J. Econ. Entomol. 47, 1045 (1954 b).

    CAS  Google Scholar 

  • Metcalf, R. L., R. B. March, and T. R. Fukuto, and M. G. Maxon: The nature and significance of Systox residues in plant materials. J. Econ. Entomol. 48, 364 (1955).

    CAS  Google Scholar 

  • Mills, P. A.: Detection and semiquantitative estimation of chlorinated organic pesticide residues in food by paper chromatography. J. Assoc. Official Agr. Chemists 42, 734 (1959).

    CAS  Google Scholar 

  • Mills, P. A.: Paragraph 221 (A). In: Pesticide analytical manual, Vol. I. U.S. Department of Health, Education and Welfare, Food and Drug Administration, Washington, D.C. (1965).

    Google Scholar 

  • Mumma, R. O., W. B. Wheeler, D. E. H. Frear, and R. H. Hamilton: Dieldrin: Extraction of accumulations by root uptake. Science 152, 530 (1966).

    Article  PubMed  CAS  Google Scholar 

  • Murphy, R. T., L. K. Gaston, and F. A. Gunther: Colorimetric analytical method for Bidrin residues in alfalfa, celery, lemon peel, lettuce, orange peel, potatoes, string beans, and tomatoes. J. Agr. Food Chem. 13, 242 (1965 a).

    Article  CAS  Google Scholar 

  • Murphy, R. T., J. R. O’Neal, W. H. Ewart, and F. A. Gunther: Persistence of Bidrin residues on and in mature oranges and in laboratory-processed citrus pulp cattle feed. J. Agr. Food Chem. 13, 550 (1965 b).

    Article  CAS  Google Scholar 

  • Rajzman, A.: Les résidus de biphényle dans les agrumes. Residue Reviews 8, 1 (1965).

    PubMed  CAS  Google Scholar 

  • Samuel, B. L., and H. K. Hodges: Screening methods for organochlorine and organophosphate insecticides in foods and feeds. Residue Reviews 17, 35 (1967).

    PubMed  CAS  Google Scholar 

  • Schnorbus, R. R., and W. F. Phillips: New extraction system for residue analysis. J. Agr. Food Chem. 15, 661 (1967).

    Article  CAS  Google Scholar 

  • Sinclair, W. B.: The orange: Its biochemistry and physiology. See especially chapter 9 by J. G. Kirchner, pp. 265 ff. Berkeley: University of California Press (1961).

    Google Scholar 

  • Souci, S. W.: Biphenyl and o-phenylphenol as postharvest fungistats in citrus fruits and citrus products. Proc. Internat. Citrus Symposium, Riverside, Calif., Mar. 16–26 (1968). In press.

    Google Scholar 

  • Souci, S. W., and G. Maier-Haarländer: Über den Diphenylgehalt und -geruch von Citrusfruchten und Citruserzeugnissen sowie den Übergang von Diphenyl auf unbehandelte Fruchte bei der Lagerung. Residue Reviews 16, 103 (1966).

    CAS  Google Scholar 

  • Stobwasser, H., B. Rademacher, and E. Lange: Einfluss von Nacherntefaktoren auf die Rückstände von Pflanzenschutzmitteln in Obst, Gemüse und einigen Sonderkulturen. Residue Reviews 22, 45 (1968).

    PubMed  CAS  Google Scholar 

  • Storherr, R. W., and R. R. Watts: Collaborative study of the ethyl acetate extraction, sweep co-distillation cleanup, and GLC determination, using six parent organophosphate pesticides. J. Assoc. Official Anal. Chemists 51, 662 (1968).

    CAS  Google Scholar 

  • Swisher, H. E.: Personal communications (Mar. and Sept. 1968).

    Google Scholar 

  • Thornburg, W. W.: Extraction and cleanup procedures. In G. Zweig (ed.): Analytical methods for pesticides, plant growth regulators, and food additives, Vol. I, pp. 87–108. New York: Academic Press (1963).

    Google Scholar 

  • Turrell, F. M.: Tables of surfaces and volumes of spheres and of prolate and oblate spheroids and spheroidal coefficients. Berkeley: University of California Press (1946).

    Google Scholar 

  • van Middelem, C. H.: Principles of residue analysis. In G. Zweig (ed.): Analytical methods for pesticides, plant growth regulators, and food additives, Vol. I, pp. 25–46. New York: Academic Press (1963).

    Google Scholar 

  • van Middelem, C. H.: Review of pesticides in Florida citrus and products. Proc. Internat. Citrus Symposium, Riverside, Calif., Mar. 16–26 (1968). In press.

    Google Scholar 

  • Wedding, R. T.: Some physiological aspects of the use of systemic insecticides. J. Agr. Food Chem. 1, 832 (1953).

    Article  CAS  Google Scholar 

  • Westlake, W. E., and F. A. Gunther: Occurrence and mode of introduction of pesticides in the environment. Adv. Chem. Series 60, 120 (1966).

    Google Scholar 

  • Westlake, W. E., and F. A. Gunther: Advances in gas chromatographic detectors illustrated from applications to pesticide residue evaluations. Residue Reviews 18, 176 (1967).

    Google Scholar 

  • Wheeler, W. B., and D. E. H. Frear: Extraction of chlorinated hydrocarbon pesticides from plant materials. Residue Reviews 16, 86 (1966).

    CAS  Google Scholar 

  • Williams, E. F.: Properties of O,O-diethyl O-p-nitrophenyl thiophosphate and O,O-diethyl O-p-nitrophenyl phosphate. Ind. Eng. Chem. 43, 950 (1951).

    Article  CAS  Google Scholar 

  • Wilson, C. W.: Personal communication (1950).

    Google Scholar 

  • Wisniewski, J. V.: Pesticide residues in marmalades and preserves. F & M Facts and Methods for Scientific Research 6(4), 3 (1965).

    Google Scholar 

  • Zweig, G. (ed.): Analytical methods for pesticides, plant growth regulators, and food additives, Vols. I to V. New York: Academic Press (1963–1967).

    Google Scholar 

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Gunther, F.A. (1969). Insecticide residues in California citrus fruits and products. In: Gunther, F.A. (eds) Residue Reviews / Rückstands-Berichte. Reviews of Environmental Contamination and Toxicology, vol 28. Springer, New York, NY. https://doi.org/10.1007/978-1-4615-8452-0_1

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