Abstract
We demonstrate cylindrical island grain bicrystals grown via a hybrid additive manufacturing/directional solidification technique. The island grain bicrystal is formed using a specialized mold in which one grain (the island) is enveloped by another larger grain (the surrounding matrix). The grain boundary plane orientation varies continuously around the circumference of the island grain, making these specimens ideal for probing grain boundary structure–property relations. We report thermal groove angle measurements along the grain boundary in a tin island grain bicrystal which show the grain boundary energy as a function of a single degree of freedom in the five-dimensional grain boundary parameter space.
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Acknowledgements
This work was supported by the George R. Brown School of Engineering at Rice University. A portion of the research used resources at the Spallation Neutron Source, a DOE Office of Science User Facility operated by the Oak Ridge National Laboratory. The authors would like to thank Baker Hughes for providing optical profilometry facilities. The authors would also like to thank Professor Srikanth Patala for his help determining the misorientation point group, as well as for his suggestions and comments.
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Ware, L.G., Herstein, B.S., Zhang, Y., Bilheux, H.Z., Cordero, Z.C. (2022). Hybrid Additive Manufacturing of Island Grain Bicrystals. In: TMS 2022 151st Annual Meeting & Exhibition Supplemental Proceedings. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-92381-5_99
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DOI: https://doi.org/10.1007/978-3-030-92381-5_99
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