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Conventional and Analytical Electron Microscopy Study of Phase Transformation in Implanted Diamond Layers

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Abstract

Graphitization of ion-beam induced amorphous layers in diamond has attracted significant interest due to ability to fabricate device structures containing two structural forms of carbon. The graphitic layers can be chemically etched to form free-standing diamond films. In the present work the graphitization process was studied using conventional and analytical transmission electron microscopy (TEM). It was found that annealing at 550 °C results in a partial graphitization of the implanted volume with graphitic phase in the middle of the amorphous layer. Annealing at 1400 °C resulted in complete graphitization of the amorphous layers.

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References

  1. A.D. Greentree et al., “Critical components for diamond-based quantum coherent devices”, J. Phys.: Condens. Matter, 18 (2006), S825–S842.

    Google Scholar 

  2. F. Jelezko et al., “Observation of Coherent Oscillation of a Single Nuclear Spin and Realization of a Two-Qubit Conditional Quantum Gate”, Phys. Rev. Let. 93 (2004), 130501–130504.

    Article  Google Scholar 

  3. P. Olivero et al., “Ion-beam-assisted lift-off technique for three-dimensional micromachining of freestanding single-crystal diamond”, Advanced Matererials, 17 (2005), 2427–2430.

    Article  Google Scholar 

  4. B. A. Fairchild et al., “Fabrication of ultrathin single-crystal diamond membranes”, Advanced Materials, 20 (2008), 4793–4798.

    Article  Google Scholar 

  5. R. Kalish et al., “Ion-implantation-induced defects in diamond and their annealing: experiment and simulation”, Phys. Stat. Sol. A, 174 (1999), 83–89.

    Article  Google Scholar 

  6. D.P. Hickey, K.S. Jones, and R.G. Elliman, “Amorphization and graphitization of single-crystal diamond _ A transmission electron microscopy study”, Diamond and Related Materials, 18 (2009) 1353–1359.

    Article  Google Scholar 

  7. J.F. Zeigler, J.P. Biersak, SRIM2008, 2008. Available from: http://www.srim.org .

    Google Scholar 

  8. S. Rubanov, and A. Suvorova “Ion implantation in diamond using 30 keV Ga focused ion beam”, Diamond and Related Materials, 20 (2011), 1160–1164.

    Article  Google Scholar 

  9. Egerton R.F. Electron Energy Loss Spectroscopy in the Electron Microscope. Plenum Press, 1996.

    Book  Google Scholar 

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© 2013 TMS (The Minerals, Metals & Materials Society)

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Rubanov, S., Fairchild, B.A., Suvorova, A., Olivero, P., Prawer, S. (2013). Conventional and Analytical Electron Microscopy Study of Phase Transformation in Implanted Diamond Layers. In: Marquis, F. (eds) Proceedings of the 8th Pacific Rim International Congress on Advanced Materials and Processing. Springer, Cham. https://doi.org/10.1007/978-3-319-48764-9_416

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