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Capillary GC with Selective Detection Using on-line Solid Phase Extraction and Liquid Chromatography Techniques

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Analysis of Pesticides in Ground and Surface Water II

Part of the book series: Chemistry of Plant Protection ((PLANT PROTECTIO,volume 12))

Abstract

Recent developments in coupling sample preparation and isolation techniques on-line to capillary gas chromatography are outlined. These developments are applied in order to enhance speed and convenience in pesticide trace analysis of tap, ground and surface water. Advantages and disadvantages of the several combination types are discussed and examples for their application in water analysis are shown. Most attention is devoted to the on-line combination of solid-phase extractions and GC using selective detection. The potential and limitations of other combinations, viz. liquid-liquid extraction-GC, solid-phase extraction-thermal desorption-GC open tubular trap-GC and solid-phase micro extraction-GC. Further technical progress may be expected in the area of on-line and automated analyte isolation combined with GC.

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References

  1. Grob K, Fröhlich D, Schilling B, Neukom H-P, Nägeli P (1984) J. Chromatogr. 295: 55

    Article  CAS  Google Scholar 

  2. Grob K Jr, Stoll J-M (1986) HRC & CC 9: 518

    Article  CAS  Google Scholar 

  3. Staniewski J, Janssen H-G, Cramers CA, Rijks JA (1992) J. Microcol. Sep. 4: 331

    Google Scholar 

  4. Vreuls JJ, de Jong GJ, Ghijsen RT, Brinkman UATh, J. Ass. Off. Anal. Chem. (in press)

    Google Scholar 

  5. Riekkola ML, J. Chromatogr. (1989) 473: 315

    Article  Google Scholar 

  6. Davies IL, Markides KE, Lee ML, Raynor MW, Bartle KD (1989) HRC 12: 193

    Article  CAS  Google Scholar 

  7. Cortes HJ, Pfeiffer CD, Jewett GL, Richter BE (1989) J. Microcol. Sep. 1: 28.

    Google Scholar 

  8. Grob K Jr, Li Z (1989) J. Chromatogr. 473: 423

    Article  Google Scholar 

  9. Grob K (1989) J. Chromatogr. 473: 73

    Google Scholar 

  10. Grob K, Müller E (1989) J. Chromatogr. 473: 411

    Article  Google Scholar 

  11. Duquet D, Dewaele C, Verzele M, McKinley M (1988) HRC & CC 11: 824

    Article  CAS  Google Scholar 

  12. Pouwelse A, de Jong D, van den Berg JHM (1988) HRC & CC 11: 607

    Article  CAS  Google Scholar 

  13. Goosens EC, de Jong D, van den Berg JHM, de Jong GJ, Brinkman UATh (1991) J. Chromatogr. 552: 489

    Article  CAS  Google Scholar 

  14. Grob K, Artho A (1991) HRC 14: 212

    Article  CAS  Google Scholar 

  15. Grob K, Li Z (1989) J. Chromatogr. 473: 381

    Article  Google Scholar 

  16. Grob K, Li Z (1989) J. Chromatogr. 473: 391

    Article  Google Scholar 

  17. Grob K, Neukom HP, Li Z (1989) J. Chromatogr. 473: 401

    Article  Google Scholar 

  18. van der Hoff GR, van Zoonen P, Grob K, HRC, in press

    Google Scholar 

  19. Hankemeier Th, Vreuls JJ, Brinkman UATh (in preparation)

    Google Scholar 

  20. Audunsson G (1988) Anal. Chem. 60: 1340

    Article  PubMed  CAS  Google Scholar 

  21. Vreuls JJ, Goudriaan VP, de Jong FJ, Brinkman UATh (1991) HRC 14: 475

    Article  CAS  Google Scholar 

  22. Roeraade J (1985) J. Chromatogr. 330: 263

    Article  CAS  Google Scholar 

  23. Fogelqvist E, Krysell M, Danielsson L-G (1986) Anal. Chem. 58: 1516

    Google Scholar 

  24. Goosens EC, Bunschooten RG, Engelen V, de Jong D, van den Berg JHM (1990) HRC 13: 438

    Article  CAS  Google Scholar 

  25. de Ruiter C, Wolf JH, Brinkman UATh, Frei RW (1987) Anal. Chim. Acta 192: 267

    Google Scholar 

  26. Goosens EC, Broekman MH, Wolters MH, Strijker RE, de Jong D, de Jong GJ, Brinkman UATh (1992) HRC 15: 242

    Article  CAS  Google Scholar 

  27. Ballesteros E, Gallego M, Valcärcel M (1993) J. Chromatogr. 633: 169

    Article  CAS  Google Scholar 

  28. van Zoonen P, van der Hoff GR, Hogendoorn EA (1990) HRC 13: 483

    Article  Google Scholar 

  29. Ogorka J, Schwinger, Bruat G (1992) J. Chromatogr. 626: 87

    Article  CAS  Google Scholar 

  30. Brouwer ER, Lingeman H, Brinkman UATh (1990) Chromatographia 29: 415

    Article  CAS  Google Scholar 

  31. Kwakman PJM, Vreuls JJ, Brinkman UATh, Ghijsen RT (1992) Chromatographia 34: 41

    Article  CAS  Google Scholar 

  32. Irth H (1989) Ligand exchange principles for trace enrichment and detection in liquid chromatography. Ph.D. Thesis, Free University, Amsterdam, the Netherlands

    Google Scholar 

  33. Farjam A, de Jong GJ, Frei RW, Brinkman UATh, Haasnoot W, Hamers ARM, Schilt R, Huf FA (1988) J. Chromatogr. 452: 419

    Article  PubMed  CAS  Google Scholar 

  34. Werkhoven-Goewie CE, Brinkman UATh, Frei RW (1981) Anal. Chem. 53: 2072

    Google Scholar 

  35. Noroozian E, Maris FA, Nielen MWF, Frei RW, de Jong GJ, Brinkman UATh (1987) HRC & CC 10: 17

    Article  CAS  Google Scholar 

  36. Noy THM, Weiss E, Herps T, Van Cruchten H, Rijks J (1988) HRC & CC 11: 181

    Article  CAS  Google Scholar 

  37. Vreuls JJ, Cuppen WJGM, Dolecka E, Maris FA, de Jong GJ, Brinkman UATh (1989) HRC 12: 807

    Article  CAS  Google Scholar 

  38. Vreuls JJ, Cuppen WJGM, de Jong GJ, Brinkman UATh (1990) HRC 13: 157

    Article  CAS  Google Scholar 

  39. Farjam A, Vreuls JJ, Cuppen WJGM, de Jong GJ, Brinkman UATh (1991) 63: 2481

    CAS  Google Scholar 

  40. Vreuls JJ, Bulterman A-J, Gnijsen RT, Brinkman UATh (1992) Analyst 117: 1701

    Article  CAS  Google Scholar 

  41. Bulterman A-J, Vreuls JJ, Ghijsen RT, Brinkman UATh (1993) HRC 16: 397

    Article  CAS  Google Scholar 

  42. Louter AJH, Brinkman UATh, Ghijsen RT (1993) Proc. 15th Symp. Capillary Chromatography, Riva del Garda, Italy, 1993, Hüthig, Heidelberg; J. Microcol. Sep. 5: 303

    Google Scholar 

  43. Louter AJH, Rinkema FD, Ghijsen RT, Brinkman UATh, Int. J. Environ. Anal. Chem., in press

    Google Scholar 

  44. Vreuls JJ, Ghijsen RT, de Jong GJ, Brinkman UATh (1992) J. Chromatogr. 625: 237

    Article  CAS  Google Scholar 

  45. Picó Y, Vreuls JJ, Ghijsen RT, Brinkman UATh, Chromatographia, in press

    Google Scholar 

  46. Picó Y, Louter AJH, Vreuls JJ, Brinkman UATh, Analyst (submitted for publication)

    Google Scholar 

  47. van der Hoff GR, Gort SM, Baumann RA, van Zoonen P (1991) HRC 14: 465

    Article  Google Scholar 

  48. Szpunar-Lobinska JS, Ceulemans M, Lobinski R, Adams FC (1993) Anal. Chim. Acta 278: 99

    Google Scholar 

  49. Schomburg G, Bastian E, Behlau H, Husmann H, Weeke F (1984) HRC & CC 7: 4

    Article  CAS  Google Scholar 

  50. Vreuls JJ, Brinkman UATh, de Jong GJ, Grob K, Artho A (1991) HRC 14: 455

    Article  CAS  Google Scholar 

  51. Vreuls JJ, Ghijsen RT, de Jong GJ, Brinkman UATh (1993) J. Microcol. Sep. 5: 317

    Google Scholar 

  52. Mol HGJ, Janssen H-GM, Cramers CA, Brinkman UATh (1993) HRC 16: 459

    Article  CAS  Google Scholar 

  53. Grob K, Schilling B (1985) HRC & CC 8: 726

    Article  CAS  Google Scholar 

  54. Kaiser RE, Rieder R (1989) J. Chromatogr. 477: 49

    Article  CAS  Google Scholar 

  55. Goretti G, Russo MV, Veschetti E (1992) HRC 15: 51

    Article  CAS  Google Scholar 

  56. Mol HGJ, Janssen H-G, Cramers CA (1993) HRC 16: 413

    Article  CAS  Google Scholar 

  57. Staniewski J, Janssen H-G, Cramers CA, Rijks JA (1992) J. Microcol. Sep. 4: 331

    Google Scholar 

  58. Mol HGJ, Staniewski J, Janssen H-G, Cramers CA, Ghijsen RT, Brinkman UATh (1993) J. Chromatogr. 630: 201

    Article  Google Scholar 

  59. Arthur CL, Pawliszyn J (1990) Anal. Chem. 62: 2145

    Google Scholar 

  60. Louch D, Motlagh S, Pawliszyn J (1992) Anal. Chem. 64: 1187

    Google Scholar 

  61. Arthur CL, Killiam LM, Buchholz KD, Pawliszyn J, Berg JR (1992) Anal. Chem. 64: 1960

    Article  CAS  Google Scholar 

  62. Arthur C, Potter D, Buchholz K, Motlagh S, Pawliszyn J (1992) LC-GC 10: 656

    CAS  Google Scholar 

  63. Potter D, Pawliszyn J (1992) J. Chromatogr. 625: 247

    Article  PubMed  CAS  Google Scholar 

  64. Arthur CL, Pratt K, Motlagh S, Pawliszyn J, Arthur CL (1992) J. Chromatogr. 603: 185

    Article  PubMed  Google Scholar 

  65. Hawthorne SB, Miller DJ, Pawliszyn J, Arthur CL (1992) J. Chromatogr. 603: 185

    Article  PubMed  CAS  Google Scholar 

  66. Page BD, Lacroix G (1993) J. Chromatogr. 648: 199

    Article  PubMed  CAS  Google Scholar 

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© 1995 Springer-Verlag Berlin Heidelberg

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Vreuls, J.J., Louter, A.J.H., Brinkman, U.A.T. (1995). Capillary GC with Selective Detection Using on-line Solid Phase Extraction and Liquid Chromatography Techniques. In: Stan, HJ. (eds) Analysis of Pesticides in Ground and Surface Water II. Chemistry of Plant Protection, vol 12. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-01063-1_1

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  • DOI: https://doi.org/10.1007/978-3-662-01063-1_1

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  • Print ISBN: 978-3-662-01065-5

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