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Dynamic compaction of calcium phosphate biomaterials

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Abstract

The purpose of this study was to apply the dynamic compaction process to calcium phosphate biomaterials. this new technique is currently used to compact metallic powders at room temperature but has not been previously applied to biomaterials. A detailed study of hydroxyapatite compacts was carried out to determine shock compaction parameters. Low static precompaction (3.1 MPa) resulted in slight peripheral cracks. A compaction degree of about 70% and macrohardness of 51 Hv were achieved for a striker velocity of about 50 m/s. FTIR spectroscopy and X-ray diffraction showed no differences in structure and composition after dynamic compaction. Two other infrequently used biomaterials were also tested: an unstable octacalcium phosphate and β-calcium metaphosphate fibres. Scanning electron microscopy showed that dynamic compaction preserved the initial fibre structure of the material. No major structural or chemical changes were noted after shock consolidation. Our results show that dynamic compaction could extend the range of bioceramics.

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References

  1. M. AKAO, H. AOKI and K. KATO, J. Mater. Sci. 16 (1981) 809.

    Google Scholar 

  2. M. JARCHO, C. H. BOLEN, M. B. THOMAS, J. BOBICK, J. F. KAY and R. H. DOREMUS, J. Mater. Sci. 11 (1976) 2027.

    Google Scholar 

  3. H. M. ROOTARE, J. M. POWERS and R. G. CRAIG, J. Dent. Res. 57 (1978) 777.

    Google Scholar 

  4. S. BEST, W. BONFIELD and C. DOYLE, in Proceedings of the 1st International Bioceramic Symposium, edited by H. Dorishi, H. Aoki and K. Sawai (Ishiyako America Inc., 1989) p. 68.

  5. A. BIGI, A. INCERTI, N. ROVERI, E. FORESTI-SERANTONI, R. MONGIORGI, L. RIVA DI SANSEVERINO, A. KRAJEWSKI and A. RAVAGLIOLI, Biomaterials 1 (1980) 140.

    Google Scholar 

  6. W. BOHNE, J. A. POUËZAT, L. PERU and G. DACULSI, Cells and Materials 3 (1993) 377.

    Google Scholar 

  7. A. KRAJEWSKI and A. RAVAGLIOLI, Biomaterials 2 (1981) 105.

    Google Scholar 

  8. M. H. ES-SAHEB, J. Mater. Sci. 27 (1992) 4151.

    Google Scholar 

  9. A. FERREIRA, M. A. MEYERS, N. N. THADHANI, S. N. CHANG and J. R. KOUGH, Metall. Trans. A 22A (1991) 685.

    Google Scholar 

  10. A. FERREIRA, M. A. MEYERS and N. N. THADHANI, Metall. Trans. A 23A (1992) 3251.

    Google Scholar 

  11. M. A. MEYERS and S. L. WANG, Acta Metall. 36 (1988) 925.

    Google Scholar 

  12. Y. MORIMOTO, T. HAYASHI and A. NAKANISHI, Inst. Phys. Conf. Series No 70, paper presented at 3rd Conf. on Mech. Prop. of High Rates of Strain, Oxford (1984).

  13. D. G. MORRIS, Metal. Sci. 15 (1981) 116.

    Google Scholar 

  14. N. W. PAGE and D. RAYBOULD, Mater. Sci. Eng. A 118 (1989) 179.

    Google Scholar 

  15. D. RAYBOULD, J. Mater. Sci. 16 (1981) 589.

    Google Scholar 

  16. D. RAYBOULD, J. Mater. Sci. 19 (1984) 3498.

    Google Scholar 

  17. T. KASUGA and Y. ABE, Phos. Res. Bull. 2 (1992) 17.

    Google Scholar 

  18. G. DACULSI, R. Z. LEGEROS, E. NERY, K. LYNCH and B. KEREBEL, J. Biomed. Mater. Res. 23 (1989) 883.

    Google Scholar 

  19. G. DACULSI, N. PASSUTI, S. MARTIN, C. DEUDON, R. Z. LEGEROS and S. RAHER, J. Biomed. Mater. Res. 23 (1990) 379.

    Google Scholar 

  20. K. DEGROOT, Biomaterials 1 (1980) 47.

    Google Scholar 

  21. C. A. VANBLITTERSWIJK, J. J. GROTE, W. KUIJPERS, W. Th. DAEMS and K. DEGROOT, Biomaterials 7 (1986) 137.

    Google Scholar 

  22. D. CLEMENT and J. FABER, in “Actualités en biomatériaux” (Romillat, Courtry, 1993) p. 152.

    Google Scholar 

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Authors and Affiliations

  1. Laboratoire de Recherche sur les Matériaux d'Intérêt Biologique, Faculté de Chirurgie Dentaire, 1 place Alexis Ricordeau, 44042, NANTES, France

    M. Trecant & G. Daculsi

  2. Laboratoire FORSEM/COMPOSITE, Institut Universitaire de Technologie, 3 rue du Maréchal Joffre, 44041, NANTES Cedex, France

    M. Leroy

Authors
  1. M. Trecant
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  2. G. Daculsi
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  3. M. Leroy
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Trecant, M., Daculsi, G. & Leroy, M. Dynamic compaction of calcium phosphate biomaterials. J Mater Sci: Mater Med 6, 545–551 (1995). https://doi.org/10.1007/BF00151037

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  • DOI: https://doi.org/10.1007/BF00151037

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