Abstract
Commercial samples of hydroxyl terminated polybutadienes (HTPB) were analysed by 1H and 13C NMR spectroscopy, in regard to hydroxylated end groups. The results were discussed and compared with those reported so far.
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References
J.A. Verdol, P.W. Ryan (ARCO Chemical Co.) — U.S. Pat. 3,714,110 (1973).
W.D. Vilar (PETROBRÁS S.A.) — Braz. Pat. 7707285 (1982).
G. Fages, Q.T. Pham — Makromol. Chem. 179, 1011–23 (1978).
Y. Camberlin, J.P. Pascault, Q.T. Pham — Makromol. Chem. 180, 397–409 (1979).
Q.T. Pham — Makromol. Chem. 182, 1167–76 (1981).
I. Deschères, O. Paissé, J.N. Colonna-Ceccaldi, Q.T. Pham — Makromol. Chem. 188 (3), 583–91 (1987).
M. Ghafari, Q.T. Pham — Makromol. Chem. 184, 1669–83 (1983).
I. Deschères, Q.T. Pham — Makromol. Chem. 191, 891–906 (1990).
Q.T. Pham — “Proton and Carbon NMR Spectra of Polymers”, Penton Press. London (1991).
K.C. Raney, M.W. Hayes, A.G. Altenau — Macromolecules 6 (5), 795–6 (1973).
L.S. Bresler, E.N. Barantsevich, V.I. Polyansky — Makromol. Chem. 183, 2479–89 (1982).
R.F. Johnson, W.C. Jankowiski — “13C NMR Spectra”, John Willey & Sons, N.Y. (1972).
SPECINFO Data Base from STN (Scientific and Technical Net Work) Data Bank (1991).
J.B. Brothers — “Carbon 13 NMR Spectroscopy”, Organic Chemistry-A Series of Monographs. Vol 24, Academic Press, N.Y (1972).
H. Inagaki, N. Donkai, A. Saitoh, Y. Zenitani — J. Appl. Polym. Sci., 28, 3741–52 (1984).
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Vilar, W.D., Menezes, S.M.C. & Akcelrud, L. Characterization of hydroxyl-terminated polybutadiene. Polymer Bulletin 33, 557–561 (1994). https://doi.org/10.1007/BF00296164
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DOI: https://doi.org/10.1007/BF00296164