Skip to main content
Log in

An interlaboratory comparison of piston-cylinder pressure calibration using the albite-breakdown reaction

  • Published:
Contributions to Mineralogy and Petrology Aims and scope Submit manuscript

Abstract

The pressure of the reaction albite=jadeite and quartz was measured at 600° C by workers in six geophysical laboratories for the purpose of comparing pressure calibration procedures for the solid-pressure piston-cylinder apparatus. All groups used the same starting mix of crystalline reactant and products and all obtained hydrothermal reversals of the equilibrium. Solid pressure media used included talc, NaCl, boron nitride, pyrophyllite, pyrex glass and crushable ceramic. Various means of calibration were used, including internal standardization by transitions in indicator substances and the piston-in, piston-out bracketing method.

There was agreement among all groups—the average preferred value of 16.3 kilobars at 600° C is enclosed by all of the error brackets assigned by the various investigators. This average preferred value is lower by nearly two kilobars than the often-quoted extrapolation of Birch and LeComte's data (1960). It will be important for both petrology and high-pressure technology to test this result in a very high gas pressure apparatus.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  • Adams, L. H.: A note on the stability of jadeite. Am. J. Sci. 251, 299–308 (1953).

    Google Scholar 

  • Bell, P. M., Mao, H. K.: Subsolidus reactions of jadeite (NaAlSi2O6) and albite (NaAlSi3O8). Ann. Rept. of the Director of the Geophys. Lab., Carnegie Inst. of Wash. Yearqook 69, 168–170 (1971).

    Google Scholar 

  • —, Rooseboom, E. H.: Phase diagram for the system nepheline-quartz. Ann. Rept. of the Director of the Geophys. Lab., Carnegie Inst. Wash. Yearbook 64, 139–141 (1965).

    Google Scholar 

  • Birch, F., LeComte, P.: Temperature-pressure plane for albite composition. Am. J. of Sci. 258, 209–215 (1960).

    Google Scholar 

  • Bobrowsky, A.: Pressure alterations through use of solid containers or jackets in high pressure environments. In: High pressure measurement, A. A. Giardini and E. C. Lloyd, eds., p. 172–185. Washington, D. C.: Butterworth 1963.

    Google Scholar 

  • Boettcher, A. L., Wyllie, P. J.: Melting of granite with excess water to 30 kilobars pressure. J. Geol. 76, 235–244 (1968a).

    Google Scholar 

  • —: The quartz-coesite transition measured in the presence of a silicate liquid and pistoncylinder calibration. Contr. Mineral. and Petrol. 17, 224–232 (1968b).

    Google Scholar 

  • —: Jadeite stability measured in the presence of silicate liquids in the system NaAlSiO4-SiO2-H2O. Geochim. Cosmochim. Acta 32, 999–1012 (1968c).

    Google Scholar 

  • Boyd, F. R., Bell, P. M., England, J. L., Gilbert, M. C.: Pressure measurement in single-stage apparatus. Ann. Rept. of the Director of the Geophys. Lab., Carnegie Inst. of Wash. Yearbook 65, 410–414 (1967).

    Google Scholar 

  • —, England, J. L.: Pyrope. Ann. Rept. of the Director of the Geophys. Lab., Carnegie Inst. of Wash. Yearbook 58, 83–87 (1959).

    Google Scholar 

  • —: Apparatus for phase equilibrium measurements at pressures up to 50 kilobars and temperatures up to 1750° C. J. Geophys. Res. 65, 741–748 (1960).

    Google Scholar 

  • —: Effect of pressure of the melting points of diopside, CaMgSi2O6, and albite, NaAlSi3O8 in the range up to 50 kilobars. J. Geophys. Res. 68, 311–323 (1963).

    Google Scholar 

  • Bridgman, P. T.: Polymorphism, principally of the elements up to 50,000 kg/cm2. Phys. Rev. 48, 893–906 (1935).

    Google Scholar 

  • —: Polymorphic transitions of 35 substances to 50,000 kg/cm2. Proc. Am. Acad. Arts and Sci. 72, 45–136 (1937).

    Google Scholar 

  • Bridgman, P. W.: Rough compressibilities of fourteen substances to 45,000 kg/cm2. Proc. Am. Acad. Arts and Sci. 72, 207–225 (1938).

    Google Scholar 

  • —: The measurement of hydrostatic pressure to 30,000 kg/cm2. Proc. Am. Acad. Arts and Sci. 74, 1–10 (1940a).

    Google Scholar 

  • —: The compression of 46 substances to 50,000 kg/cm2. Proc. Am. Acad. Arts and Sci. 74, 21–51 (1940b).

    Google Scholar 

  • Clark, S. P.: Effect of pressure on the melting points of eight alkali halides. J. Chem. Phys. 31, 1526–1531 (1959).

    Google Scholar 

  • Coes, L. Jr.: A new dense crystalline silica. Science 118, 131–132 (1953).

    Google Scholar 

  • Corll, J. A.: Experimental verification of pressure enhancement by encapsulation. J. Appl. Phys. 38, 2707–2709 (1967).

    Google Scholar 

  • Green, D. H., Ringwood, A. E.: An experimental investigation of the gabbro to eclogite transformation and its petrological applications. Geochim. Cosmochim. Acta 31, 767–833 (1967).

    Google Scholar 

  • Green, T. H., Ringwood, A. E., Major, A.: Friction effects and pressure calibration in a piston-cylinder apparatus at high pressure and temperature. J. Geophys. Res. 71, 3589–3994 (1966).

    Google Scholar 

  • Haygarth, J. C., Getting, I. C., Kennedy, G. C.: Determination of the pressure of the barium 1–11 transition with a single-stage piston-cylinder apparatus. J. Appl. Phys. 38, 4557–4564 (1967).

    Google Scholar 

  • Hill, R. E. T., Boettcher, A. L.: Water in the earth's mantle: melting curves of basalt-water and basalt-water-carbon dioxide. Science 167, 980–982 (1970).

    Google Scholar 

  • Hlabse, T., Kleppa, O. J.: The thermochemistry of jadeite. Am. Mineralogist 53, 1281–1292 (1968).

    Google Scholar 

  • Jamieson, J. C., Olinger, B.: (in press.) Pressure inhomogeneity—a possible source of error in using internal standards for pressure gauges, in Proceedings of a Symposium on Accurate Characterization of the High Pressure Environment, National Bureau of Standards. Gaithersburg, Maryland.

  • Johannes, W., Puhan, D.: The calcite-aragonite transition, reinvestigated. Contr. Mineral. and Petrol. 31, 28–38 (1971).

    Google Scholar 

  • Kelley, K. K., Todd, S. S., Orr, R. L., King, E. G., Bonnicksen, K. R.: Thermodynamic properties of sodium-aluminum and potassium-aluminum silicates. U. S. Bur. Mines Rept. of Invest. 4955 (1953).

  • Kracek, F. C., Neuvonen, K. J., Burley, G.: Thermochemistry of mineral substances I: A thermodynamic study of jadeite. J. Wash. Acad. Sci. 41, 373–383 (1953).

    Google Scholar 

  • Kushiro, I., Yoder, H. S.: Anorthite-forsterite and anorthite-enstatite reactions and their bearing on the basalt-eclogite transformation. J. Petrol. 7, 337–362 (1966).

    Google Scholar 

  • Luedemann, H. D., Kennedy, G. C.: Melting curves of lithium, sodium, potassium and rubidium to 80 kilobars. J. Geophys. Res. 73, 2795–2805 (1968).

    Google Scholar 

  • Newton, M. S., Kennedy, G. C.: Jadeite, analcite, nepheline and albite at high temperatures and pressures. Am. J. Sci. 266, 728–735 (1968).

    Google Scholar 

  • Newton, R. C.: The thermal stability of zoisite. J. Geol. 73, 431–441 (1965).

    Google Scholar 

  • —: Some calc-silicate equilibrium relations. Am. J. Sci. 264, 204–222 (1966).

    Google Scholar 

  • —, Kennedy, G. C.: Some equilibrium relations in the join CaAl2Si2O8-H2O. J. Geophys. Res. 68, 2967–2983 (1963).

    Google Scholar 

  • —, Smith, J. V.: Investigations concering the breakdown of albite at depth in the earth. J. of Geol. 75, 268–286 (1967).

    Google Scholar 

  • Parsons, C. A.: Experiments on carbon at high temperatures and under great pressures, and in contact with other substances. Proc. Royal Soc. 44, 320–323 (1888).

    Google Scholar 

  • Richardson, S. W., Bell, P. M., Gilbert, C. M.: Kyanite-sillimanite equilibrium between 700° and 1500° C. Am. J. Sci. 266, 513–541 (1968).

    Google Scholar 

  • Yoder, H. S., Tilley, C. E.: Origin of basalt magmas: An experimental study of natural and synthetic rock systems. J. Petrol. 3, 342–532 (1962).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Johannes, W., Bell, P.M., Mao, H.K. et al. An interlaboratory comparison of piston-cylinder pressure calibration using the albite-breakdown reaction. Contr. Mineral. and Petrol. 32, 24–38 (1971). https://doi.org/10.1007/BF00372231

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00372231

Keywords

Navigation