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GC-MS and HPLC analyses of lignin degradation products in biomass hydrolyzates

GC-MS- und HPLC-Analytik von Ligninabbauprodukten in Biomassehydrolysaten

  • Original Papers
  • Biomass Hydrolyzates
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Fresenius' Zeitschrift für analytische Chemie Aims and scope Submit manuscript

Zusammenfassung

Die gas-chromatographische Trennung von Ligninabbauprodukten nach hydrolytischer Spaltung von Biomasse (z.B. Pappelholz) sowie die massenspektrometrische Identifizierung werden beschrieben. Für eine routinemäßige Analytik der Ligninabbauprodukte in Biomassehydrolysaten wird weiterhin die Trennung mittels einer Gradienten-HPLC-Methode aufgezeigt. Die Detektion erfolgte bei 280 nm. Neben Referenzproben wurden hydrothermale Abbaulösungen untersucht.

Summary

The gas-chromatographic separation of lignin degradation products of hydrolytically degraded biomass (e. g. poplar wood) and their mass spectrometric identification are described. For routine analysis of lignin degradation products of biomass hydrolyzates, a time saving HPLC gradient method using a UV-detection system (280 nm), is described. In addition to reference samples, solutions of hydrothermally degraded biomass were analyzed.

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Authors and Affiliations

  1. Institute for Radiochemistry, University of Innsbruck, Innrain 52a, A-6020, Innsbruck, Austria

    R. Pecina, P. Burtscher, G. Bonn & O. Bobleter

Authors
  1. R. Pecina
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  2. P. Burtscher
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  3. G. Bonn
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  4. O. Bobleter
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Pecina, R., Burtscher, P., Bonn, G. et al. GC-MS and HPLC analyses of lignin degradation products in biomass hydrolyzates. Z. Anal. Chem. 325, 461–465 (1986). https://doi.org/10.1007/BF00489135

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  • DOI: https://doi.org/10.1007/BF00489135

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