Skip to main content
SpringerLink
Log in

X-ray structure of 3,3′-bis(4-methylthioquinolinyl) sulfide

  • Published:
Journal of Crystallographic and Spectroscopic Research Aims and scope Submit manuscript

Abstract

The structure of the title compound has been solved by direct methods, and refined to anR value of 0.035 for 1613 reflections. Both methyl carbon atoms deviate from the plane of the pyridine ring by 1.505(3) Å in opposite directions. Both sulfur atoms S(1) and S(2) remain in short contact, at 3.247(1) Å. The two pyridine rings are inclined at 61.4(2)° to each other.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  • Baranowska, I., Karmiński, W., Baranowski, R. (1973)Microchim. Acta, 815.

  • Boryczka, S., Wyszomirski, M., Maślankiewicz, A., Borowiak, T., and Kubicki, M. (1990)Recl. Trav. Chim., Pay-Bas 109, 509.

    Google Scholar 

  • Maślankiewicz, A. (1985)Polish J. Chem. 59, 511.

    Google Scholar 

  • Maślankiewicz, A., and Pluta, K. (1980)Polish J. Chem. 54, 33.

    Google Scholar 

  • Maślankiewicz, A., Wyszomirski, M., and Gkl/owiak, T. (1990)J. Cryst. Spectr. Res. 20, 375.

    Google Scholar 

  • Pauling, L. (1960)The Nature of the Chemical Bond (third edition) (Cornell, Ithaca).

    Google Scholar 

  • Pluta, K. (1990) manuscript in preparation.

  • Syntex (1976)XTL Structure Determination System (Syntex Analytical Instruments, Cupertino, Calif.).

    Google Scholar 

  • Sheldrick, G. (1986)Shelxs 86; Program for crystal solution (Univ. Gottingen, Germany).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Organic Chemistry, Silesian School of Medicine, Jagiellońska Street 4, 41-200, Sosnowiec, Poland

    Krystian Pluta & Andrzej Maślankiewicz

  2. Institute of Chemistry, University of Wrocław, F. Joliot-Curie Street 14, 50-383, Wrocław, Poland

    Tadeusz Głowiak

Authors
  1. Krystian Pluta
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Andrzej Maślankiewicz
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Tadeusz Głowiak
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Part XIV in the series of Azinyl Sulfides.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Pluta, K., Maślankiewicz, A. & Głowiak, T. X-ray structure of 3,3′-bis(4-methylthioquinolinyl) sulfide. Journal of Crystallographic and Spectroscopic Research 21, 153–156 (1991). https://doi.org/10.1007/BF01161057

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01161057

Keywords

Search

Navigation