Skip to main content
Log in

Analytical electron microscopy of internally oxidized low Si-Al steel

  • Published:
Metallurgical Transactions A Aims and scope Submit manuscript

Abstract

Analytical electron microscopy was used to study the precipitates in internally oxidized low Si-Al steels, of the type used for electric motor laminations. After oxidizing heat treatments of one and five hours at 788 °C, the internally precipitated particles were about 0.1 to 0.2 μm in diameter. At the internal-oxidation reaction front, thin plates of Al2O3 precipitated. Subsequently, a shell of SiO2 precipitated on the Al2O3 core. Depth of internal oxidation was predicted from the knowledge of precipitate composition, treatment time and temperature, and published information.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. G. P. Huffman and E. B. Stanley:J. Appl. Phys., 1979, vol. 50, pp. 2363–65.

    Article  ADS  CAS  Google Scholar 

  2. A. L. Geiger:J. Appl. Phys., 1979, vol. 50, pp. 2366–68.

    Article  ADS  CAS  Google Scholar 

  3. G. Lyudkovsky, A. G. Preban, and J. M. Shapiro:J. Appl. Phys., 1982, vol. 53, pp. 2419–21.

    Article  ADS  CAS  Google Scholar 

  4. R. A. Rapp:Corrosion, 1965, vol. 21, pp. 382–401.

    CAS  Google Scholar 

  5. J. H. Swisher:Oxidation of Metals and Alloys, ASM, Metals Park, OH, 1971, pp. 235–67.

    Google Scholar 

  6. J. L. Meijering:Advances in Materials Research, Wiley-Interscience, New York, NY, 1971, pp. 1–81.

    Google Scholar 

  7. J. Takada, K. Kashiwagi, and M. Adachi:J. Matls. Sci., 1984, vol. 19, pp. 3451–58.

    Article  CAS  Google Scholar 

  8. J. Takada and M. Adachi:J. Matls. Sci., 1986, vol. 21, pp. 2133–37.

    Article  CAS  Google Scholar 

  9. W. L. Block and N. Jayaraman:Matl. Sci. and Tech., 1986, vol. 2, pp. 22–27.

    CAS  Google Scholar 

  10. A. Zidek and Z. Huliciova:Hutnicke Listy, 1972, vol. 27, pp. 424–28.

    CAS  Google Scholar 

  11. J. Takada, S. Yamamoto, S. Kikuchi, and M. Adachi:Oxidation of Metals, 1986, vol. 25, pp. 93–105.

    Article  CAS  Google Scholar 

  12. J. Takada, S. Yamamoto, S. Kikuchi, and M. Adachi:Metall. Trans. A, 1986, vol. 17A, pp. 221–29.

    CAS  Google Scholar 

  13. M. T. Hepworth, R. P. Smith, and E. T. Turkdogan:Trans. TMSAIME, 1966, vol. 236, pp. 1278–82.

    CAS  Google Scholar 

  14. J. H. Swisher and E. T. Turkdogan:Trans. TMS-AIME, 1967, vol. 239, pp. 426–31.

    CAS  Google Scholar 

  15. S. A. Bradford:Trans. TMS-AIME, 1964, vol. 230, pp. 1400–05.

    CAS  Google Scholar 

  16. R. Kiessling and N. Lange:Non-Metallic Inclusion in Steel, MSP 194, The Metals Society, London, 1978, Part I.

    Google Scholar 

  17. M. Tinker and P. A. Lebon:Oxidation of Metals, 1982, vol. 18, pp. 27–40.

    Article  CAS  Google Scholar 

  18. R. C. Gifkins:J. Aust. Inst. Met., 1976, vol. 21, pp. 175–77.

    CAS  Google Scholar 

  19. G. Cliff and G. W. Lorimer:J. Micros., 1975, vol. 103, pp. 203–11.

    Google Scholar 

  20. G. Cliff, D. M. Maher, and D. C. Joy:J. Micros., 1984, vol. 136, pp. 219–25.

    CAS  Google Scholar 

  21. L. W. Hobbs and M. R. Pascucci:Journal de Physique, Colloque C6, 1980, vol. 41, pp. 237–42.

    Google Scholar 

  22. M. R. Pascucci, J. L. Hutchinson, and L. W. Hobbs:Radiation Effects, Gordon and Breach, 1983, pp. 219–26.

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Michael, J.R., Stephenson, E.T. Analytical electron microscopy of internally oxidized low Si-Al steel. Metall Trans A 19, 953–959 (1988). https://doi.org/10.1007/BF02628380

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02628380

Keywords

Navigation