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Chemical and micro-structural changes in glass-like carbon during high temperature heat treatment

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Abstract

A glass-like carbon was fabricated using furan resin. The influence of heat treatment temperature during fabrication process on the chemical and micro-structural changes was studied by various analytical and spectroscopic methods including TGA, FT-IR, CHN, TEM and XRD. The chemical resistance properties of the fabricated glasslike carbon were also investigated. It has been found that the heat-treated samples at higher temperature up to 2600 °C in N2 atmosphere had little weight loss, small amounts of functional groups, and high carbon content. The fabricated glass-like carbons upon heat treatment at 2600 °C showed an amorphous stage without any grain growth and/or reconstruction of structure. The glass-like carbon had much better chemical resistance than the artificial graphite, and exhibited a high chemical resistance due to its low surface areas, minimum impurities, and low graphite crystallites.

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Authors and Affiliations

  1. Department of Ceramic Engineering, Myongji University, Yongin, 449-728, Kyunggi-do, Korea

    Yun-Soo Lim, Hee-Seok Kim & Myung-Soo Kim

  2. Department of Materials Science and Engineering, Inha University, 402-751, Incheon, Korea

    Nam-Hee Cho

  3. Department of Materials Science and Engineering, Korea University, 136-701, Seoul, Korea

    Sahn Nahm

Authors
  1. Yun-Soo Lim
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  2. Hee-Seok Kim
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  3. Myung-Soo Kim
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  4. Nam-Hee Cho
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  5. Sahn Nahm
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Lim, YS., Kim, HS., Kim, MS. et al. Chemical and micro-structural changes in glass-like carbon during high temperature heat treatment. Macromol. Res. 11, 122–127 (2003). https://doi.org/10.1007/BF03218341

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  • DOI: https://doi.org/10.1007/BF03218341

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