Skip to main content
Log in

A characterization method for mechanical properties of metal powder bed fusion parts

  • ORIGINAL ARTICLE
  • Published:
The International Journal of Advanced Manufacturing Technology Aims and scope Submit manuscript

Abstract

The main objective of this research is to develop a characterization method for parts fabricated in metal powder bed fusion (PBF) processes, a type of additive manufacturing (AM) process. To characterize conventionally manufactured parts, many methods and standards are available, while no comprehensive standards or methods are available for AM parts. In this paper, a mechanical property characterization method is proposed that involves statistical analysis to select sample sizes and test coupon design considerations for metal printing, printing parameters, and applicability of existing testing standards for metal PBF, in addition to several mechanical properties. As proof of concept for the proposed characterization method, material and mechanical property characterization of the metal printed (EOS M280) EOS maraging steel grade 300 material is presented along with selected sample lots and relative errors. The characterization method presented in this paper is applicable to any metal AM process.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12

Similar content being viewed by others

Abbreviations

A, B:

Specimen notation for printed and heat-treated samples, respectively

DED:

Directed energy deposition

e :

Maximum acceptable sampling error, also called allowable relative error

S :

Maximum acceptable difference between the true and sample means

n :

Number of data points

PBF:

Powder bed fusion

σ :

Standard deviation

X :

Data from test results

\( \overline{X} \) :

The mean of the data

References

  1. Gibson DR, Stucker B (2015) Additive manufacturing technologies; 3D printing, rapid prototyping, and direct digital manufacturing, 2nd Ed. Springer, New York

    Google Scholar 

  2. ISO 17296-3:2014, Additive manufacturing -- general principles -- part 3: main characteristics and corresponding test methods, 2014

  3. Slotwinski J, Moylan S (2014) Applicability of existing materials testing standards for additive manufacturing materials, NISTIR 8005, National Institute of Standards and Technology, U.S Department of Commerce

  4. ASTM F3122-14, ASTM International, 2014

  5. Yasa E, Kempen K, Kruth J, Thijs, Humbeeck J (2010) Microstructure and mechanical properties of maraging steel 300 after selective laser sintering, in The 21st Annual International Solid Freefrom Fabrication Symposium- An Additive Manufacturing conference, Austin, Texas

  6. Du W, Bai Q, Zhang B (2018) Machining characteristics of 18Ni-300 steel in additive/substractive hybrid manufacturing. Int J Adv Manuf Technol 95:2509–2519

    Article  Google Scholar 

  7. Fortunato A, Lulaj A, Melkote S, Liverani E, Ascari A, Umbrello D (2018) Milling of maraging steel components produced by selective laser melting. Int J Adv Manuf Technol 95:1895–1902

    Article  Google Scholar 

  8. Guo Z, Sha W (2004) Modelling the correlation between processing parameters and properties of maraging steels using artificial neural network. Comput Mater Sci 29:12–28

    Article  Google Scholar 

  9. Demir, Previtsli B (2017) Investigation of remelting and preheating in SLM of 18Ni300 maraging steel as corrective and preventive measures for porosity reduction. Int J Adv Manuf Technol 93:2697–2709

    Article  Google Scholar 

  10. Monkova K, Zetkova I, Kucerova L, Zetek M, Monka P, Dana M (2018) Study of 3D printing direction and effects of heat treatment on mechanical properties of MS1 maraging steel, Arch Appl Mech

  11. EOS, Material data sheet, EOS GmbH-Electro Optical Systems, 2011

  12. Suryawanshi J, Prashanth K, Ramamurthy U (2017) Tensile, fracture, and fatigue crack growth properties of a 3D printed maraging steel through selective laser melting. J Alloys Compd 725:355–364

    Article  Google Scholar 

  13. ASTM, ASTM E122–17: standard sample size to estimate, with specified precision, the average for a characteristic of a lot or process, ASTM international, 2017

  14. EOS, Machine and Software Parameters EOSINT M280, EOS GmbH-Electro Optical Systems, 2014

  15. Yao Y, Huang Y, Chen B, Tan C, Su Y, Feng J (2018) Influence of processing parameters and heat treatment on the mechanical properties of 18Ni300 manufactured by laser based directed energy deposition. Opt Laser Technol:171–179

  16. EOS, Operation-EOSINT M280-Laser-Sintering system for metal powder, Munchen: EOS

  17. Bai Y, Yang Y, Wang D, Zhang M (2017) Influence mechanism of parameters process and mechanical properties evolution mechanism of maraging steel 300 by selective laser melting. Mater Sci Eng A:116–123

  18. Yasa E, Deckers J, Kruth J, Rombouts M, Luyten J (2010) Charpy impact testing of metallic selective laser melting parts. Virtual Phys Prototyping:89–98

  19. Branco R, Costa J, Berto F, Javad Razavi S, Martins Ferreria J, Capela C, Santos L and Antunes F (2018) Low-cycle fatigue behaviour of AISI 18Ni300 maraging steel produced by selective laser melting, Metals, vol. 8, no. 32

  20. Hermann Becker T, Dimitrov D (2016) The achieveable mechanical properties of SLM produced maraging steel 300 components, Rapid Prototyp J, pp. 487–494

  21. ASTM (2016) ASTM-E8-16a, standard test methods for tension testing of metallic materials, West Conshohocken: ASTM International

  22. ASTM (2016) ASTM-E23-16b, standard test methods for notched bar impact testing of metallic materials, West Conshohocken, Pennsylvania: ASTM International

  23. ASTM (2017) ASTM E18-17e1, standard test methods for Rockwell hardness of metallic materials, West Conshohocken, PA: ASTM International

  24. ASTM (2011) ASTM E3-11, standard practice for preparation of metallographic specimens, ASTM International

  25. ASTM (2017) ASTM B311-17, standard test method for density of powder metallurgy (PM) materials containing less than two percent porosity, PA: ASTM International

  26. Tan C, Zhou K, Ma W, Zhang P, Liu M, Kuang T (2017) Microstructural evolution, nanoprecipitation behaviour and mechanical properties of selective laser melted high-performance grade 300 maraging steel. Mater Des 134:23–34

    Article  Google Scholar 

  27. Aboulkhair NT, Everitt NM, Ashcroft I, Tuck C (2014) Reducing porosity in AlSi10Mg parts processed by selective melting. Addit Manuf 1-4:77–86

    Google Scholar 

Download references

Acknowledgments

The authors would like to thank the funding agency, NAMIC (National Additive Manufacturing and Innovation Center) through grant 2017295, partner ST Engineering Land Systems, Singapore, for their in-kind contributions. Authors acknowledge the efforts of Senior Specialist Mr. Kai Lee, Digital Manufacturing and Design Centre, SUTD, Singapore, for assistance with specimen fabrication and testing.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to David W. Rosen.

Additional information

Publisher’s note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Raju, N., Kim, S. & Rosen, D.W. A characterization method for mechanical properties of metal powder bed fusion parts. Int J Adv Manuf Technol 108, 1189–1201 (2020). https://doi.org/10.1007/s00170-020-05298-7

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00170-020-05298-7

Keywords

Navigation