Skip to main content
Log in

Quantitative Determination of Density and Mass of Polymeric Materials Using Microfocus Computed Tomography

  • Published:
Journal of Nondestructive Evaluation Aims and scope Submit manuscript

Abstract

A density calibration of homogeneous polymeric materials in the range of 0.9 to 2.2 g/cm3 with micro Computed Tomography (CT) scanning was devised and its accuracy, repeatability and potential sources of error were investigated. The density of unknown materials could be determined successfully in many cases with this calibration. However, in some cases the experimental values deviated significantly from the actual values. These deviations could be attributed mainly to chemical compositional differences compared to the calibration materials. Dual energy CT could be used to determine whether a material is within the range of atomic composition of the calibration materials, in which case the calibration function is accurate. If a material is outside the chemical composition range determined by dual energy CT, the calibration is not applicable and accurate density cannot be determined.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7

References

  1. Mull, R.T.: Mass estimated by computed tomography: physical density from CT numbers. Am. J. Roentgenol. 143(5), 1101–1104 (1984)

    Article  Google Scholar 

  2. Philips, D.H., Lannutti, J.J.: Measuring physical density with X-ray computed tomography. Nondestruct. Test. Eval. Int. 30(6), 339–350 (1997)

    Google Scholar 

  3. Lang, T.F., Li, J., Harris, S.T., Genant, H.K.: Assessment of vertebral bone mineral density using volumetric quantitative CT. J. Comput. Assist. Tomogr. 23(1), 130–137 (1999)

    Article  Google Scholar 

  4. Zou, W., Hunter, N., Swain, M.V.: Application of polychromatic μCT for mineral density determination. J. Dent. Res. 90(1), 18–30 (2011)

    Article  Google Scholar 

  5. Lindgren, L.O.: Medical CAT scanning: X-ray absorption coefficients, CT numbers and their relation to wood density. Wood Sci. Technol. 25, 341–349 (1991)

    Google Scholar 

  6. Freyburger, C., Longuetaud, F., Mothe, F., Constant, T., Leban, J.-M.: Measuring wood density by means of X-ray computer tomography. Ann. For. Sci. 66, 804 (2009)

    Article  Google Scholar 

  7. Macedo, A., Vaz, C.M.P., Pereira, J.C.D., Naime, J.M., Cruvinel, P.E., Crestana, S.: Wood density determination by X- and gamma-ray tomography. Holzforschung 56, 535–540 (2002)

    Article  Google Scholar 

  8. Stoel, B.C., Borman, T.M., de Jongh, R.: Wood densitometry in 17th and 18th century Dutch, German, Austrian and French violins, compared to classical cremonese and modern violins. PLoS ONE 7(10), e46629 (2012)

    Article  Google Scholar 

  9. Meincken, M., du Plessis, A.: Visualising and quantifying thermal degradation of wood by computed tomography. Eur. J. Wood Prod. (2013)

  10. Sasov, A.: X-ray microtomography of plastics and composite materials. In: Bonse, U. (ed.) Proceedings of SPIE, Developments in X-Ray Tomography III, vol. 4503, pp. 274–281 (2001)

    Chapter  Google Scholar 

  11. Schilling, P.J., Karedla, B.R., Tatiparthi, A.K., Verges, M.A., Herrington, P.D.: X-ray computed microtomography of internal damage in fiber reinforced polymer matrix composites. Compos. Sci. Technol. 65, 2071–2078 (2005)

    Article  Google Scholar 

  12. Cho, Z.H., Tsai, C.M., Wilson, G.: Study of contrast and modulation mechanisms in X-ray/photon transverse axial transmission tomography. Phys. Med. Biol. 20(6), 879–889 (1975)

    Article  Google Scholar 

Download references

Acknowledgements

Stellenbosch University and National Research Foundation funding was used in this project. The CT scanner was granted by the National Research Foundation through the National Equipment Program. We acknowledge useful comments from reviewers in a previous version of this manuscript.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to A. du Plessis.

Rights and permissions

Reprints and permissions

About this article

Cite this article

du Plessis, A., Meincken, M. & Seifert, T. Quantitative Determination of Density and Mass of Polymeric Materials Using Microfocus Computed Tomography. J Nondestruct Eval 32, 413–417 (2013). https://doi.org/10.1007/s10921-013-0195-7

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10921-013-0195-7

Keywords

Navigation