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Effect of process parameters on the synthesis of mesoporous nanocrystalline zirconia with triblock copolymer as template

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Abstract

Nanocrystalline zirconia powders with high surface area, mesoporous structure and tetragonal crystallite phase have been prepared by the surfactant-assisted route by using of Pluronic P123 block copolymer surfactant. The effect of several process parameters such as the type of zirconium precursor, pH value, refluxing time, refluxing temperature and surfactant to zirconium molar ratio on the structural properties of the powders have been investigated.

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Authors and Affiliations

  1. Chemical Engineering Department, University of Kashan, 87317-51167, Kashan, Iran

    M. Rezaei

  2. Chemical Engineering Department, Iran University of Science and Technology, P.O. Box 16315-67, Tehran, Iran

    S. M. Alavi

  3. Petrochemical Research & Technology Company (NPC-RT), Tehran, Iran

    S. Sahebdelfar

  4. State Key Laboratory for Heavy Oil Processing, Key Laboratory of Catalysis, CNPC, China University of Petroleum, Dongying, 257061, China

    Zi-Feng Yan

Authors
  1. M. Rezaei
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  2. S. M. Alavi
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  3. S. Sahebdelfar
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  4. Zi-Feng Yan
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Correspondence to Zi-Feng Yan.

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Rezaei, M., Alavi, S.M., Sahebdelfar, S. et al. Effect of process parameters on the synthesis of mesoporous nanocrystalline zirconia with triblock copolymer as template. J Porous Mater 15, 171–179 (2008). https://doi.org/10.1007/s10934-007-9120-8

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  • DOI: https://doi.org/10.1007/s10934-007-9120-8

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