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Synthesis and characterization of MCM-41-type composite materials prepared from ZSM-5 zeolite

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Abstract

Micro/mesoporous composite materials with microporous and mesoporous double pores-size distribution were hydrothermally synthesized by using slurry or filtrate of alkali-treated ZSM-5 zeolite and were characterized by XRD, N2 adsorption, FT-IR, TEM and so on. The XRD and TEM patterns indicate the composite materials possess ordered hexagonal structure. The sample MZ-B using filtrate of alkali-treated ZSM-5 zeolite hardly contains raw ZSM-5 particles. However, sample MZ-A originated from the slurry of alkali-treated ZSM-5 zeolite may contain some ZSM-5 crystallites, owing to the differences in concentration and time of alkaline treatment for ZSM-5 zeolite.

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Authors and Affiliations

  1. State Key Laboratory for Heavy Oil Processing, Key Laboratory of Catalysis, CNPC, China University of Petroleum, Dongying, 257061, China

    Chun-Min Song, Jie Jiang & Zi-feng Yan

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  1. Chun-Min Song
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  2. Jie Jiang
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  3. Zi-feng Yan
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Correspondence to Zi-feng Yan.

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Song, CM., Jiang, J. & Yan, Zf. Synthesis and characterization of MCM-41-type composite materials prepared from ZSM-5 zeolite. J Porous Mater 15, 205–211 (2008). https://doi.org/10.1007/s10934-007-9121-7

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  • DOI: https://doi.org/10.1007/s10934-007-9121-7

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