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Effect of Bonding Time on Dissimilar Transient Liquid Phase (TLP) Bonding of IN939 to IN625 Superalloys: Microstructural Characterization and Mechanical Properties

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Abstract

The microstructure and mechanical properties of transient liquid phase (TLP) bonded joints between dissimilar precipitation hardened IN939 and solid solution hardened IN625 with a Ni-Cr-Si-Fe-B filler alloy were studied. The TLP bonding was conducted in different bonding times (i.e., 15, 25, 35, 45, 60, and 90 minutes). Different phases, formed in the isothermally solidified zone (ISZ), on-cooling solidified zone, and diffusion affected zone (DAZ), were characterized using EDS, XRD, and EPMA analyses. A Ni-rich γ solid solution, CrB, and Ni3B were detected in the centerline of samples with incomplete isothermal solidification (i.e., 15 and 25 minutes), formed by binary and ternary eutectic reactions. Raising the time of bonding boosted isothermal solidification, resulting in a joint without deleterious eutectic microconstituents in bonding times of 35 minutes and higher. Chromium-rich borides were discovered in the DAZ of IN939, while the IN625-DAZ side was composed of chromium-molybdenum-rich borides. The concentration of alloying elements in the ISZ experienced an increment by further raising the bonding time to 90 minutes, creating a more homogenous bond with increased ISZ microhardness and mechanical properties. The highest shear strength (~ 92 and ~ 77 Pct that of the IN939 and IN625, respectively) and failure energy were attained for the 90-minutes sample. The fracture mechanism was also switched from a brittle semi-cleave morphology to a more ductile dimple-like morphology by increasing the bonding time from 15- to 90-minutes.

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Authors and Affiliations

  1. The Institute for Future Transport and Cities, Coventry University, Coventry, CV1 5FB, UK

    Amirhossein Sadeghian

  2. Department of Materials and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), Tehran, 15875-4413, Iran

    Amirhossein Sadeghian, Seyyed Ehsan Mirsalehi & Farzam Arhami

  3. Department of Mechanical, Industrial and Aerospace Engineering (MIAE), Concordia University, Montreal, H3G 1M8, Canada

    Farzam Arhami

  4. Ceramic Division, Materials and Energy Research Center, Tehran, 14155-4777, Iran

    Ahmad Malekan

  5. Department of Materials Science and Engineering, Kyushu University, 744, Motooka, Nishi-ku, Fukuoka, 819-0395, Japan

    Noritaka Saito & Kunihiko Nakashima

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  1. Amirhossein Sadeghian
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  2. Seyyed Ehsan Mirsalehi
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Correspondence to Seyyed Ehsan Mirsalehi.

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Manuscript submitted September 19, 2020; accepted January 31, 2021.

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Sadeghian, A., Mirsalehi, S.E., Arhami, F. et al. Effect of Bonding Time on Dissimilar Transient Liquid Phase (TLP) Bonding of IN939 to IN625 Superalloys: Microstructural Characterization and Mechanical Properties. Metall Mater Trans A 52, 1526–1539 (2021). https://doi.org/10.1007/s11661-021-06176-x

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