Abstract
Powder injection molding (PIM) is an advanced manufacturing technology with advantages including shape complexity, high production rate, and high physical/mechanical properties. However, because PIM has many sub-steps, such as mixing, injection molding, debinding, and sintering, the optimization of each process condition is important to avoid defects including warpage, crack, and blister. In this paper, the warpage, one of the most common defects in PIM, is investigated by using thin square copper structures with lengths of 10 mm and thicknesses of 600 and 190 μm. The warpage of each structure is measured by using a white light interferometric surface profiler. The measured warpage of the structure fabricated by the standard process is 3.771 μm. When the solvent debinding step is absent, the warpage becomes 8.052 μm. Additionally, sensitivity analysis determines that the effect of the thermal debinding step’s heating rate is dominant to warp the structure. Normalized sensitivities of the debinding heating rates are 0.58 for the structure with a thickness of 600 μm and 0.63 for the other structure. Finally, how to optimize the processing condition is outlined.
Graphic Abstract
Similar content being viewed by others
References
R.M. German, A. Bose, Injection Molding of Metals and Ceramics, 1st edn. (Metal Power Industries Federation, New Jersey, 1997), pp. 11–54
L. Liu, N.H. Loh, B.Y. Tay, S.B. Tor, Y. Murakoshi, R. Maeda, Acta Mater. 56, 5560 (2008)
J.W. Oh, W.S. Lee, S.J. Park, Metals Mater. Int. 24, 142 (2018)
H. Cho, J. Godinez, J.S. Han, D. Fadda, S.M. You, J. Lee, S.J. Park, Materials 12, 507 (2019)
W.J. Tseng, J. Mater. Process. Technol. 102, 14 (2000)
J. Meng, N.H. Loh, G. Fu, S.B. Tor, B.Y. Tay, J. Alloys Compd. 496, 293 (2010)
W.J. Tseng, D.M. Liu, Ceram. Int. 24, 125 (1998)
S.G. Li, G. Fu, I. Reading, S.B. Tor, N.H. Loh, P. Chaturvedi, S.F. Yoon, K. Youcef-Toumi, Appl. Phys. A 89, 721 (2007)
A. Keshavarz Panahi, H. Mianajiy, E. Miandoabchi, M. Hussaini Fareed, J. Manuf. Sci. Eng. 135, 011006 (2013)
V. Friederici, M. Ellerhorst, P. Imgrund, S. Krämer, N. Ludwig, Powder Metall. 57, 5 (2014)
H. Zhang, X. He, X. Qu, L. Zhao, Mater. Sci. Eng. A 526, 31 (2009)
C. Wang, Z. Lu, K. Zhang, Materials 11, 1864 (2018)
L. Poh, C. Della, S. Ying, C. Goh, Y. Li, Powder Technol. 328, 256 (2018)
C. Veeresh Nayak, G.C. Manjunath Patel, M.R. Ramesh, V. Desai, S.K. Samanta, Materials Forming, Machining and Post Processing, 1st edn. (Springer, Cham, 2019), pp. 41–74
C.W. Gal, S.S. Han, J.S. Han, D. Lin, S.J. Park, Int. J. Appl. Ceram. Technol. 16, 315 (2019)
R.M. German, A. Bose, Injection Molding of Metals and Ceramics, 1st edn. (Metal Power Industries Federation, New Jersey, 1997), pp. 175–218
R.M. German, A. Bose, Injection Molding of Metals and Ceramics, 1st edn. (Metal Power Industries Federation, New Jersey, 1997), pp. 219–264
B. Ozcelik, I. Sonat, Mater. Design 30, 367 (2009)
H.T. Lim, S.H. Kim, H.D. Im, K.H. Oh, S.H. Jeong, J. Micromech. Microeng. 18, 105013 (2008)
G. Zhou, J. Li, L. Lv, Appl. Thermal Eng. 109, 514 (2016)
R.M. German, A. Bose, Injection Molding of Metals and Ceramics, 1st edn. (Metal Power Industries Federation, New Jersey, 1997), pp. 99–132
J. Raja, V. Radhakrishnan, Wear 57, 147 (1979)
S.V. Atre, S.J. Park, R. Zauner, R.M. German, Powder Metall. 50, 76 (2007)
J.H. Jeong, S.K. Ryu, S.J. Park, H.C. Shin, J.-H. Yu, Comput. Mater. Sci. 100, 21 (2015)
Z. Shi, Z.X. Guo, J.H. Song, Acta Mater. 50, 1937 (2002)
D. Lin, S.T. Chung, Y.S. Kwon, S.J. Park, J. Mech. Sci. Technol. 30, 1859 (2016)
H.E. Kissinger, Anal. Chem. 29, 1702 (1957)
S.J. Park, Y. Wu, D.F. Heaney, X. Zou, G. Gai, R.M. German, Metall. Mater. Trans. A 40, 215 (2009)
Acknowledgements
This work was supported by POSCO and the National Research Foundation of Korea (NRF) Grant (NRF-2019R1A2C3003129) funded by the Ministry of Science and ICT (MSIT), Republic of Korea.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
The authors declare that they have no conflict of interest.
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Cho, H., Park, J.M., Rho, J. et al. Warpage of Powder Injection Molded Copper Structure. Met. Mater. Int. 27, 1131–1137 (2021). https://doi.org/10.1007/s12540-019-00492-z
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s12540-019-00492-z