Abstract
Equal-channel angular pressing (ECAP) was applied on AM90 magnesium alloy using processing route \(\hbox {B}_{\mathrm {C}}\) at \(275\,^\circ \)C up to four passes. Microstructural evolution and the corresponding modification in mechanical properties (strength, elongation and hardness) corresponding to the number of ECAP passes were evaluated using X-ray diffraction (XRD), electron backscatter diffraction, scanning electron microscopy, transmission electron microscopy, tensile test and microhardness test. Shear deformation was found to refine the microstructure by breaking it into smaller grains formed by dislocation reconstruction. Tensile strength and hardness were found to increase by \(\sim \)128 and 23%, respectively, for ECAP-processed 2-pass sample in comparison with that of the homogenized condition. After two passes, tensile strength and hardness started decreasing even though the grain size was still decreasing, which was found to be associated with texture modification during ECAP processing as observed by XRD analysis.
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References
Hu, H.; Yu, A.; Li, N.; Allison, J.E.: Potential magnesium alloys for high temperature die cast automotive applications: a review. Mater. Manuf. Process. 18(5), 687–717 (2003)
Kulekci, M.K.: Magnesium and its alloys applications in automotive industry. Int. J. Adv. Manuf. Technol. 39(9), 851–865 (2008)
Sakintuna, B.; Lamari-Darkrim, F.; Hirscher, M.: Metal hydride materials for solid hydrogen storage: a review. Int. J. Hydrog. Energy 32(9), 1121–1140 (2007)
Lowe, T.C.; Valiev, R.Z.: The use of severe plastic deformation techniques in grain refinement. JOM 56(10), 64–68 (2004)
Estrin, Y.; Vinogradov, A.: Extreme grain refinement by severe plastic deformation: a wealth of challenging science. Acta Mater. 61(3), 782–817 (2013)
Ranaware, P.G.; Rathod, M.J.: Combined effect of shot peening, subcritical austenitic nitriding and cryo-treatment on surface modification of AISI 4140 steel. Mater. Manuf. Process. 32, 349–354 (2016). doi:10.1080/10426914.2016.1221112
Sekhar, K.C.; Kashyap, B.P.; Sangal, S.: A process of notch wavy rolling for strengthening metal sheets. Mater. Manuf. Process. 31(6), 781–786 (2016)
Shin, D.H.; Park, J.J.; Kim, Y.S.; Park, K.T.: Constrained groove pressing and its application to grain refinement of aluminum. Mater. Sci. Eng. A 328(1), 98–103 (2002)
Yadav, P.C.; Sinhal, A.; Sahu, S.; Roy, A.; Shekhar, S.: Microstructural inhomogeneity in constrained groove pressed Cu–Zn alloy sheet. J. Mater. Eng. Perform. 25(7), 2604–2614 (2016)
Furukawa, M.; Horita, Z.; Nemoto, M.; Langdon, T.G.: Review: processing of metals by equal-channel angular pressing. J. Mater. Sci. 36(12), 2835–2843 (2001)
Valiev, R.Z.; Langdon, T.G.: Principles of equal-channel angular pressing as a processing tool for grain refinement. Prog. Mater. Sci. 51(7), 881–981 (2006)
Surendarnath, S.; Sankaranarayanasamy, K.; Ravisankar, B.: A comparative study of commercially pure aluminum processed by ECAP using conventional and new die. Mater. Manuf. Process. 29(10), 1172–1178 (2014)
Zhu, Y.T.; Lowe, T.C.; Jiang, H.; Huang, J.: Method for producing ultrafine-grained materials using repetitive corrugation and straightening. U.S. Patent No. 6197129 B1, (2001)
Sunil, B.R.: Repetitive corrugation and straightening of sheet metals. Mater. Manuf. Process. 30(10), 1262–1271 (2015)
Zhilyaev, A.P.; Langdon, T.G.: Using high-pressure torsion for metal processing: fundamentals and applications. Prog. Mater. Sci. 53(6), 893–979 (2008)
Choi, I.C.; Lee, D.H.; Ahn, B.; Durst, K.; Kawasaki, M.; Langdon, T.G.; Jang, J.I.: Enhancement of strain-rate sensitivity and shear yield strength of a magnesium alloy processed by high-pressure torsion. Scr. Mater. 94, 44–47 (2015)
Huot, J.: High-pressure torsion. In: Enhancing Hydrogen Storage Properties of Metal Hydrides: Enhancement by Mechanical Deformations, p. 11. Springer, Switzerland (2016)
Jahedi, M.; Paydar, M.H.: Study on the feasibility of the torsion extrusion (TE) process as a severe plastic deformation method for consolidation of Al powder. Mater. Sci. Eng. A 527(20), 5273–5279 (2010)
Khosravifard, A.; Jahedi, M.; Yaghtin, A.H.: Three dimensional finite element study on torsion extrusion processing of 1050 aluminum alloy. Trans. Nonferrous Met. Soc. China 22(11), 2771–2776 (2012)
Ivanisenko, Y.; Kulagin, R.; Fedorov, V.; Mazilkin, A.; Scherer, T.; Baretzky, B.; Hahn, H.: High pressure torsion extrusion as a new severe plastic deformation process. Mater. Sci. Eng. A 664, 247–256 (2016)
Huang, H.; Tang, Z.; Tian, Y.; Jia, G.; Niu, J.; Zhang, H.; Pei, J.; Yuan, G.; Ding, W.: Effects of cyclic extrusion and compression parameters on microstructure and mechanical properties of Mg–1.50Zn–0.25Gd alloy. Mater. Des. 86, 788–796 (2015)
Tian, Y.; Huang, H.; Yuan, G.; Ding, W.: Microstructure evolution and mechanical properties of quasicrystal-reinforced Mg–Zn–Gd alloy processed by cyclic extrusion and compression. J. Alloys Compd. 626, 42–48 (2015)
Jung, K.H.; Kim, Y.B.; Lee, G.A.; Lee, S.; Kim, E.Z.; Choi, D.S.: Formability of ZK60A magnesium alloy determined by compression and backward extrusion. Mater. Manuf. Process. 29(2), 115–120 (2014)
Faraji, G.; Jafarzadeh, H.: Accumulative torsion back (ATB) processing as a new plastic deformation technique. Mater. Manuf. Process. 27(5), 507–511 (2012)
Nakamura, K.; Neishi, K.; Kaneko, K.; Nakagaki, M.; Horita, Z.: Development of severe torsion straining process for rapid continuous grain refinement. Mater. Trans. 45(12), 3338–3342 (2004)
Liao, W.; Ye, B.; Zhang, L.; Zhou, H.; Guo, W.; Wang, Q.; Li, W.: Microstructure evolution and mechanical properties of SiC nanoparticles reinforced magnesium matrix composite processed by cyclic closed-die forging. Mater. Sci. Eng. A 642, 49–56 (2015)
Guo, W.; Wang, Q.D.; Li, W.Z.; Zhosu, H.; Zhang, L.; Liao, W.J.: Enhanced microstructure homogeneity and mechanical properties of AZ91-SiC nanocomposites by cyclic closed-die forging. J. Compos. Mater. 51, 681–686 (2016). doi:10.1177/0021998316651126
Saito, Y.; Utsunomiya, H.; Tsuji, N.; Sakai, T.: Novel ultra-high straining process for bulk materials-development of the accumulative roll-bonding (ARB) process. Acta Mater. 47(2), 579–583 (1999)
Raei, M.; Toroghinejad, M.R.; Jamaati, R.: Nano/Ultrafine Structured AA1100 by ARB Process. Mater. Manuf. Process. 26(11), 1352–1356 (2011)
Yu, H.L.; Lu, C.; Tieu, A.K.; Kong, C.: Fabrication of nanostructured aluminum sheets using four-layer accumulative roll bonding. Mater. Manuf. Process. 29(4), 448–453 (2014)
Eto, M.; Sasaki, T.; Fukushima, S.; Shibahara, T.; Miyata, K.; Wakita, M.: Development of super short interval multi-pass rolling technology for ultra fine-grained hot strip. Rev. Met. Paris 103(7–8), 319–325 (2006)
Etou, M.; Fukushima, S.; Sasaki, T.; Haraguchi, Y.; Miyata, K.; Wakita, M.; Tomida, T.; Imai, N.; Yoshida, M.; Okada, Y.: Super short interval multi-pass rolling process for ultrafine-grained hot strip. ISIJ Int. 48(8), 1142–1147 (2008)
Fu, M.W.; Yong, M.S.; Pei, Q.X.; Hng, H.H.: Deformation behavior study of multi-pass ECAE process for fabrication of ultrafine or nanostructured bulk materials. Mater. Manuf. Process. 21(5), 507–512 (2006)
Valder, J.; Rijesh, M.; Surendranathan, A.O.: Forming of tubular commercial purity aluminum by ECAP. Mater. Manuf. Process. 27(9), 986–989 (2012)
Nieh, T.; Wadsworth, J.: Hall–Petch relation in nanocrystalline solids. Scr. Metll. et Mater. 25(4), 955–958 (1991)
Yoon, E.Y.; Yoo, J.H.; Yoon, S.C.; Kim, Y.K.; Baik, S.C.; Kim, H.S.: Analyses of route Bc equal channel angular pressing and post-equal channel angular pressing behavior by the finite element method. J. Mater. Sci. 45(17), 4682–4688 (2010)
Avedesian, M.M.; Baker, H.: ASM Specialty Handbook: Magnesium and Magnesium Alloys. ASM International, Ohio (1999)
Watanabe, K.; Matsuda, K.; Gonoji, T.; Kawabata, T.; Sakakibara, K.; Sanpei, Y.; Saikawa, S.; Ikeno, S.: Effect of casting method and Al contents on microstructure in AM-type magnesium alloys. Mater. Sci. Forum 654, 663–666 (2010)
Namdar, M.; Jahromi, S.A.J.: Influence of ECAP on the fatigue behavior of age-hardenable 2xxx aluminum alloy. Int. J. Miner. Metall. Mater. 22(3), 285–291 (2015)
Li, Z.; Zhou, S.J.; Huang, N.: Effects of ECAE processing temperature on the microstructure, mechanical properties, and corrosion behavior of pure Mg. Int. J. Miner. Metall. Mater. 22(6), 639–647 (2015)
Liu, T.; Zhang, W.; Wu, S.D.; Jiang, C.B.; Li, S.X.; Xu, Y.B.: Mechanical properties of a two-phase alloy Mg–8%Li–1% Al processed by equal channel angular pressing. Mater. Sci. Eng. A 360(1–2), 345–349 (2003)
Jahadi, R.; Sedighi, M.; Jahed, H.: ECAP effect on the micro-structure and mechanical properties of AM30 magnesium alloy. Mater. Sci. Eng. A 593, 178–184 (2014)
Iwahashi, Y.; Wang, J.; Horita, Z.; Nemoto, M.; Langdon, T.G.: Langdon, Principle of equal-channel angular pressing for the processing of ultra-fine grained materials. Scr. Mater. 35(2), 143–146 (1996)
Vaid, A.; Mittal, K.; Sahu, S.; Shekhar, S.: Controlled evolution of coincidence site lattice related grain boundaries. Trans. Indian Inst. Met. 69(9), 1745–1753 (2016)
Semiatin, S.L.; Jonas, J.J.: Formability and Workability of Metals: Plastic Instability and Flow Localization. American Society for Metals p. 299 (1984)
Feng, X.M.; Ai, T.T.: Microstructure evolution and mechanical behavior of AZ31 Mg alloy processed by equal-channel angular pressing. Trans. Nonferrous Met. Soc. China 19(2), 293–298 (2009)
Lin, H.K.; Huang, J.C.; Langdon, T.G.: Relationship between texture and low temperature superplasticity in an extruded AZ31 Mg alloy processed by ECAP. Mater. Sci. Eng. A 402(1), 250–257 (2005)
Jafarian, H.; Livar, J.H.; Razavi, S.H.: Microstructure evolution and mechanical properties in ultrafine grained Al/TiC composite fabricated by accumulative roll bonding. Compos. B 77, 84–92 (2015)
Chino, Y.; Kimura, K.; Mabuchi, M.: Twinning behavior and deformation mechanisms of extruded AZ31 Mg alloy. Mater. Sci. Eng. A 486, 481–488 (2008)
Austin, A.E.; Richard, N.A.: Grain-boundary diffusion. J. Appl. Phys. 32(8), 1462–1471 (1961)
Zhu, S.Q.; Yan, H.G.; Chen, J.H.; Wu, Y.Z.; Liu, J.Z.; Tian, J.: Effect of twinning and dynamic recrystallization on the high strain rate rolling process. Scr. Mater. 63(10), 985–988 (2010)
Koike, J.; Kobayashi, T.; Mukai, T.; Watanabe, H.; Suzuki, M.; Maruyama, K.; Higashi, K.: The activity of non-basal slip systems and dynamic recovery at room temperature in fine-grained AZ31B magnesium alloys. Acta Mater. 51(7), 2055–2065 (2003)
Mukai, T.; Yamanoi, M.; Watanabe, H.; Higashi, K.: Ductility enhancement in AZ31 magnesium alloy by controlling its grain structure. Scr. Mater. 45, 89–94 (2001)
Hilpert, M.; Stycznki, A.; Kiese, J.; Wanger, L.: Magnesium Alloys and Their Application. Werkstoff-informations Gesellshaft, Hamburg (1998)
Akbaripanah, F.; Fereshteh-Saniee, F.; Mahmudi, R.; Kim, H.K.: Microstructural homogeneity, texture, tensile and shear behavior of AM60 magnesium alloy produced by extrusion and equal channel angular pressing. Mater. Des. 43, 31–39 (2013)
Kim, H.K.; Kim, W.J.: Microstructural instability and strength of an AZ31 Mg alloy after severe plastic deformation. Mater. Sci. Eng. A 385(1), 300–308 (2004)
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We would like to thank Dr. Shashank Shekhar, Assistant Professor, IIT Kanpur, India, for his support in providing the laboratory facilities which helped us to carry out this work.
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Gopi, K.R., Shivananda Nayaka, H. & Sahu, S. Microstructural Evolution and Strengthening of AM90 Magnesium Alloy Processed by ECAP. Arab J Sci Eng 42, 4635–4647 (2017). https://doi.org/10.1007/s13369-017-2574-3
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DOI: https://doi.org/10.1007/s13369-017-2574-3