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Properties of Ni0.5Zn0.5Fe2O4 nanoparticles with the spinel structure synthesized via cryo-chemical method

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Abstract

Ni0.5Zn0.5Fe2O4 nanoparticles (NPs) with the spinel structure were synthesized by the cryo-chemical method with further heat treatment in the temperature range of 200–800 °C. Crystalline NPs began to form in one-stage and the degree of crystallinity grew with the increase of the heating temperature. Particles sizes, their size distributions and magnetization also tended to growth directly with the increasing the heating temperature of NPs. Magnetic fluids based on the obtained Ni0.5Zn0.5Fe2O4 NPs demonstrated effective and self-controlled heating up to the certain temperatures under the effect of an alternating magnetic field in contrast to known in literature Fe3O4 NPs with the spinel structure, which heated up uncontrolled to the extremely high phase transition temperature.

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Acknowledgements

This work was supported by the NAS of Ukraine in the framework of Target Program of Scientific Researches of the NAS of Ukraine “Grants of the NAS of Ukraine to research laboratories/groups of young scientists of the NAS of Ukraine” No 0121U110363 (2021–2022), common Ukrainian-Slovak joint research project. This work was also supported by the Slovak Academy of Sciences and Ministry of Education in the framework of project VEGA 2/0011/20, Slovak Research and Development Agency under the Contract No. APVV-18-0160. The authors acknowledge the CERIC-ERIC Consortium in the frame of Grant No 20197154 and the Romanian Ministry of Research and Innovation (from FEDR-POC No. 332/390008/29.12.2020—SMIS 109522) for the access to experimental facilities and possibility to perform HR TEM measurements.

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Authors and Affiliations

  1. V. I. Vernadsky Institute of General and Inorganic Chemistry of the NAS of Ukraine, Palladina ave., 32/34, Kyiv, 03142, Ukraine

    I. Timashkov, Y. Shlapa & A. Belous

  2. National Institute of Materials Physics, 405A Atomistilor St, 077125, Magurele, Romania

    V. A. Maraloiu

  3. Institute of Experimental Physics of Slovak Academy of Science, Watsonova 47, 040 01, Kosice, Slovakia

    M. Rajnak & M. Timko

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  1. I. Timashkov
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  2. Y. Shlapa
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  6. A. Belous
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Correspondence to Y. Shlapa.

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Timashkov, I., Shlapa, Y., Maraloiu, V.A. et al. Properties of Ni0.5Zn0.5Fe2O4 nanoparticles with the spinel structure synthesized via cryo-chemical method. Appl. Phys. A 127, 650 (2021). https://doi.org/10.1007/s00339-021-04795-0

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