Abstract
A novel vibrating finger viscometer for high-temperature measurement in liquid metals and alloys up to 1823 K was constructed. The dynamic viscosity (\(\eta \)) of the liquid fluid is measured as a product of \((\rho \cdot \eta )^{0.5}\) and the relative change of the field coil input for a constant amplitude recording at the resonant frequency of the oscillator. The viscometer was calibrated at 298 K using reference silicon oils with varying kinematic viscosities (\(\nu \)), \((0.79\hbox { to } 200)\times 10^{-6}\hbox { m}^{2}\cdot \hbox {s}^{-1}\). In the present study, the viscosity of liquid gold (\(99.99\,\%\) Au), silver (\(99.9\, \%\) Ag), and tin (\(99.9\,\%\) Sn) was measured. The viscosities expressed as an Arrhenius function of temperature are:
The viscosity values are consistent within the range of available literature data.
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K.C. Mills, L. Courtney, R.F. Brooks, B.J. Monaghan, ISIJ Int. 40, S120 (2000)
R.F. Brooks, A.T. Dinsdale, P.N. Quested, Meas. Sci. Technol. 16, 354 (2005)
Z. Morita, T. Iida, M. Kawamoto, A. Mori, Tetsu–Hagane J. Iron Steel Inst. Jpn. 70, 1242 (1984)
T. Iida, R.I.L. Guthrie, The Physical Properties of Liquid Metals (Clarendon Press, Oxford, 1993)
J. Klostermann, R. Schwarze, M. Weider, C. Brücker, Steel Res. Int. 82, 1113 (2011)
C.G. Aneziris, W. Schärfl, H. Biermann, U. Martin, Int. J. Appl. Ceram. Technol. 6, 727 (2009)
A. Jahn, K.-P. Steinhoff, T. Dubberstein, P. Franke, M. Weider, S. Wolf, A. Kovalev, A. Glage, A. Weiß, W. Schärfl, K. Eigenfeld, L. Krüger, P.R. Scheller, Steel Res. Int. 85, 477 (2014)
E.W. Washburn, Phys. Rev. 17, 273 (1921)
T. Dubberstein, M. Schürmann, H.-P. Heller, H. Chaves, Patent DE102014015301 B3, (2015)
C. Solomons, M.S. White, Trans. Faraday Soc. 65, 305 (1969)
S. Salon, V. Armenio, A. Crise, J. Fluid Mech. 570, 253 (2007)
H. Schlichting, K. Gersten, Grenzschicht-Theorie (Springer, Berlin, 2006)
B.L. Jensen, B.M. Sumer, J. Fredsøe, J. Fluid Mech. 206, 265 (1989)
T. Iida, M. Kawamoto, S. Fujimoto, Z. Morita, Tetsu–Hagane J. Iron Steel Inst. Jpn. 71, 1490 (1985)
T. Dubberstein, H.-P. Heller, Adv. Eng. Mater. 15, 583 (2013)
E. Gebhardt, G. Wörwag, Z. Für Met. 41, 358 (1951)
J. Brillo, I. Egry, H.S. Giffard, A. Patti, Int. J. Thermophys. 25, 1881 (2004)
M.J. Assael, A.E. Kalyva, K.D. Antoniadis, R.M. Banish, I. Egry, J. Wu, E. Kaschnitz, W.A. Wakeham, High Temp.–High Press. 41, 161 (2012)
M.J. Assael, A.E. Kalyva, K.D. Antoniadis, R. Michael Banish, I. Egry, J. Wu, E. Kaschnitz, W.A. Wakeham, J. Phys. Chem. Ref. Data 39, 033105 (2010)
Wacker Siliconöle AK, Wacker-Chemie GmbH, 4405 1.02 (2001)
T. Dubberstein, H.-P. Heller, High Temp.-High Press. 1, 393–406 (2014)
M. Kehr, Aufbau Eines Hochtemperaturviskosimeters Und Messung Der Viskosität von Schmelzen Des Systems Aluminium–Nickel (2009)
E. Gebhardt, M. Becker, Z. Für Met. 41, 111 (1951)
T. Iida, Z. Morita, S. Takeuchi, Nippon Kinzoku Gakkaishi J. Jpn. Inst. Met. 39, 1169 (1975)
L. Martin-Garin, R. Martin-Garin, P. Desré, J. Common Met. 59, P1 (1978)
H. Schenck, M.G. Frohberg, K. Hoffmann, Arch. Für Eisenhüttenwes. 34, 93 (1963)
T. Iida, T. Kumada, M. Washio, Z. Morita, Nippon Kinzoku Gakkai-Si 44, 1392 (1980)
M. Kehr, W. Hoyer, I. Egry, Int. J. Thermophys. 28, 1017 (2007)
W. Menz, F. Sauerwald, Acta Metall. 14, 1617 (1966)
T. Gancarz, Z. Moser, W. Gąsior, J. Pstruś, H. Henein, Int. J. Thermophys. 32, 1210 (2011)
Y. Plevachuk, V. Sklyarchuk, W. Hoyer, I. Kaban, J. Mater. Sci. 41, 4632 (2006)
Acknowledgments
This work was financially supported by the German Research Foundation (DFG) within the Collaborative Research Centre SFB 799 (TRIP-Matrix-Composite) at the Institute of Iron and Steel Technology IEST, TU Bergakademie Freiberg, which is hereby gratefully acknowledged. The authors also acknowledge the technician at IEST strongly supporting the construction of the new viscometer.
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This article is part of the selected papers of the 20th European Conference for Thermophysical Properties.
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Dubberstein, T., Schürmann, M., Chaves, H. et al. A Novel Vibrating Finger Viscometer for High-Temperature Measurements in Liquid Metals and Alloys. Int J Thermophys 37, 100 (2016). https://doi.org/10.1007/s10765-016-2104-7
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DOI: https://doi.org/10.1007/s10765-016-2104-7