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Analysis and characterization of magneto-structural transformations and critical exponent analysis of La0.8Ca0.2−xPbxMnO3

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Abstract

Because of their significant magnetocaloric properties, Ca and Pb-doped LaMnO3 can be employed in magnetic refrigeration systems. The partial substitution effect of Ca2+ by Pb2+ cations on the structural, magnetocaloric properties, and critical behavior of mixed valence perovskites La0.8Ca0.2−xPbxMnO3 (0 ≤ x ≤ 0.15), synthesized by the flash combustion route, was studied in this work. The presence of structural transformations of the prepared ceramics from an orthorhombic structure (Pbnm space group) for samples with x ≤ 0.05 to a rhombohedral system (\(R\stackrel{-}{3}c\) space group) for x ≥ 0.1 was detected by X-ray diffraction analysis, which is related to the A-site disorder. The field-cooled (FC) magnetization indicated a second-order ferromagnetic-paramagnetic transition for the investigated samples when the temperature was increased. Due to the change in the Mn3+/Mn4+ ratio, substituting Ca2+ with larger Pb2+ ions increases the Curie temperature (TC) by increasing Pb doping content from 90 K for x = 0 to 205 K for x = 0.15. The magnetization isotherms of all samples showing a second-order phase transition were studied, where an applied magnetic field of 5 T, the value of maximum magnetic entropy variation \({/\varDelta \text{S}}_{\text{M}}^{\text{m}\text{a}\text{x}}/\) for the sample with x = 0.15 was estimated to be 2.73 Jkg−1 K−1. In addition, it has a significant relative cooling power of about 276 Jkg−1 under the same applied magnetic field strength. The critical behavior of the samples was investigated close to TC. The exponent values were identical to the mean-field method, indicating a large disorder of spin magnetic moments in the perovskite compounds.

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Funding

S. Ait Bouzid acknowledges the Moroccan National Center for Scientific and Technical Research for Excellence scholarship number 17USMS2018. This work was supported through the Core Program within the National Research Development and Innovation Plan 2022–2027, carried out with the support of MCID, project no. 27 N / 03.01.2023, component project code PN 23 24 01 03.

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Authors and Affiliations

  1. Chemical Processes and Applied Materials Team, Polydisciplinary Faculty, Sultan Moulay Slimane University, B.P 523, 23000, Beni-Mellal, Morocco

    Sara Ait Bouzid & Abdellatif Essoumhi

  2. Energy and Materials Engineering Laboratory, Faculty of Sciences and Techniques, Sultan Moulay Slimane University, B.P 523, 23000, Beni-Mellal, Morocco

    Mohammed Sajieddine & Abdelhamid El Boubekri

  3. National School of Applied Sciences, Sultan Moulay Slimane University, Khouribga, Morocco

    Mohammed Sajieddine

  4. Univ. Grenoble Alpes, CNRS, Grenoble INP, Institut Néel, 38000, Grenoble, France

    El kebir Hlil

  5. National Institute of Materials Physics, Atomistilor 405A, 077125, Magurele, Ilfov, Romania

    Arpad Mihai Rostas

  6. National Institute of Isotopic and Molecular Technologies, Donat 67-103, 400293, Cluj-Napoca, Romania

    Arpad Mihai Rostas

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  1. Sara Ait Bouzid
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  2. Mohammed Sajieddine
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  3. El kebir Hlil
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  4. Abdelhamid El Boubekri
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  6. Abdellatif Essoumhi
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Contributions

SAB: Conceptualization, Visualization, Methodology, Resources, Writing—original draft, Formal analysis, Validation. MS: Supervision, Project administration, Conceptualization, Investigation, Resources, Formal analysis, Writing—review & editing, Validation. EkH: Investigation, Resources. AMR:Investigation, Resources, Writing—review & editing. AE: Supervision, Project administration, Conceptualization, Visualization, Methodology, Resources, Writing—review & editing, Validation.

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Correspondence to Sara Ait Bouzid or Abdellatif Essoumhi.

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Ait Bouzid, S., Sajieddine, M., Hlil, E.k. et al. Analysis and characterization of magneto-structural transformations and critical exponent analysis of La0.8Ca0.2−xPbxMnO3. J Mater Sci: Mater Electron 34, 2166 (2023). https://doi.org/10.1007/s10854-023-11475-7

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