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Elaboration and Experimental Investigation of Zn-Ni-Co Spinel Ferrite Multi-doped Rare-Earth (Gd, Er, and Sm) Prepared by Coprecipitation Method

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Abstract

For the first time, rare-earth multi-doped Zn-Ni-Co spinel ferrite nanoparticles \({Zn}_{0.2}{Ni}_{0.3}{Co}_{0.5}{Fe}_{(2-x-y-z)}{Er}_{x}{Gd}_{y}{Sm}_{z}{O}_{4}\) (x = 0.1, y = 0.2, z = 0.1) were synthesized by the coprecipitation method in this paper. The thermal behavior of the obtained precipitate (uncalcined powder) was studied by thermogravimetric analysis. A single phase with space group Fd \(\overline{3 }\) m was confirmed by X-ray diffraction (XRD) and the average crystallite size was found to be 16 nm. The estimation of the cationic distribution indicates a mixed spinel structure. The effect of the rare-earth elements on the nanoparticles’ morphology was evaluated by transmission electron microscopy (TEM) analysis. Magnetic measurements were performed at three different temperatures 5, 80, and 300 K, and show a superparamagnetic behavior with a saturation magnetization of 21 emu/g at room temperature and a ferromagnetic behavior at 5 K. The saturation magnetization value obtained was interpreted by exchange interactions due to the presence of rare-earth elements in our structure. Therefore, the nanoparticles prepared in this work may be promising candidates for practical applications such as high-frequency electromagnetic interference (EMI) suppression, electronics, communication, and future gigahertz antenna applications.

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Authors and Affiliations

  1. LRIT Laboratory, Associated Unit To CNRST (URAC29), IT Rabat Center, Faculty of Sciences in Rabat, Mohammed V University, Rabat, Morocco

    Y. Belaiche, K. Minaoui & M. Ouadou

  2. Nanoscience and Nanotechnology Unit, E.N.S Rabat, Energy Research Centre, Mohammed V University, B.P. 5118 Takaddoum, Rabat, Morocco

    Y. Mouhib & M. Elansary

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  1. Y. Belaiche
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  2. K. Minaoui
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  3. M. Ouadou
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  4. Y. Mouhib
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Belaiche, Y., Minaoui, K., Ouadou, M. et al. Elaboration and Experimental Investigation of Zn-Ni-Co Spinel Ferrite Multi-doped Rare-Earth (Gd, Er, and Sm) Prepared by Coprecipitation Method. J Supercond Nov Magn 35, 1269–1280 (2022). https://doi.org/10.1007/s10948-022-06189-6

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