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Synthesis, characterization, and application of CoFe2O4@TRIS@sulfated boric acid nanocatalyst for the synthesis of 2-amino-3-cyanopyridine derivatives

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Abstract

The aim of this research is the synthesis of a novel acidic nanocatalyst using the layer-by-layer assembly technique. The CoFe2O4@TRIS@sulfated boric acid nanoparticles were easily synthesized and studied as a highly beneficial, recyclable, and magnetite nanocatalyst for the synthesis of 2-amino-3-cyanopyridine derivatives. The chemical structure of CoFe2O4@TRIS @sulfated boric acid nanocatalyst was completely confirmed with different techniques like FESEM, Map, EDS, XRD, TGA/DTG, VSM, and FT-IR analyses. Briefly, the newly synthesized nanocatalyst offers some advantages such as simplicity of work-up, highly stable, environmental friendliness, reusability, excellent yields, and short reaction time.

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Acknowledgements

The authors would like to thank the Research Council of University of Sistan and Baluchestan because of its financial supporting.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, University of Sistan and Baluchestan, P.O. Box 98135-674, Zahedan, Iran

    Homayoun Faroughi Niya, Nourallah Hazeri, Malek Taher Maghsoodlou & Maryam Fatahpour

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  1. Homayoun Faroughi Niya
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  2. Nourallah Hazeri
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  3. Malek Taher Maghsoodlou
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  4. Maryam Fatahpour
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Correspondence to Nourallah Hazeri.

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Faroughi Niya, H., Hazeri, N., Maghsoodlou, M.T. et al. Synthesis, characterization, and application of CoFe2O4@TRIS@sulfated boric acid nanocatalyst for the synthesis of 2-amino-3-cyanopyridine derivatives. Res Chem Intermed 47, 1315–1330 (2021). https://doi.org/10.1007/s11164-020-04369-4

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