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Thermal and Mechanical Studies of Cerium Molybdenum Borosilicate Glasses and Glass–Ceramics

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Abstract

This investigation will focus on a particular molybdenum borosilicate glass with the form 61B2O3 – 19SiO2- (20-x) MoO3—x CeO2, x = (0 ≤ x ≤ 12 mol. %). DTA examination was conducted using a Shimadzu -DTA equipment. The powder glass samples (10 mg) were placed in a platinum pan and heated to 800 °C in nitrogen medium at various rates. The temperatures of the glass transition, \({{\varvec{T}}}_{{\varvec{g}}}\), the crystallization extrapolated onset, \({{\varvec{T}}}_{{\varvec{c}}}\), the crystallization peak, \({{\varvec{T}}}_{{\varvec{P}}}\), and melting \({{\varvec{T}}}_{{\varvec{m}}}\), were determined. The quantity of CeO2 in the checked glass had a significant impact on its crystallization behavior, with an increase in CeO2 content increasing ΔT and thus making the glasses more stable. With increasing CeO2 concentrations, both EG & Ec values decrease, as expected given the rise in \({{\varvec{T}}}_{{\varvec{g}}}\) & \({{\varvec{T}}}_{{\varvec{P}}}\) values. XRD and SEM were used to identify the crystallizing phases and microstructural morphology for each composition. Based on XRD observations, Molybdenum Silicide (Mo3Si2), Molybdenum Boride (B2Mo1), Cerium Borate (B1Ce1O3), Cerium Molybdenum Oxide (Ce16Mo21O56) and Cerium Silicide Oxide (Ce10O3Si8) phases were detected. The presence of particles with different shapes in both compositions was revealed by SEM micrographs. As CeO2 concentrations increased, the ultrasonic velocities & elastic moduli increased.

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Acknowledgements

This work was supported by the King Khalid University through grant RCAMS/KKU/04-22 under the Research Center for Advance Materials (RCAMS) at King Khalid University, Saudi Arabia. The authors express their gratitude to princess Nourah bint Abdulrahman University, Researchers Supporting Project (Grant No. PNURSP2023R32) Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia.

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Authors and Affiliations

  1. Chemistry Department, Faculty of Science, Al-Azhar University, P.O. Box 71524, Assiut, Egypt

    Kh. S. Shaaban

  2. Physics Department, College of Science, Princess Nourah Bint Abdulrahman University, P.O. Box 84428, Riyadh, 11681, Saudi Arabia

    B. M. Alotaibi

  3. Physics Department, College of Science, Jouf University, P.O. Box: 2014, Sakaka, Saudi Arabia

    Z. A. Alrowaili

  4. Department of Physics, Sakarya University, Sakarya, Turkey

    M. S. Al-Buriahi

  5. Physics Department, Faculty of Science, Islamic University, P. O. Box 170, Al Madinah, Saudi Arabia

    A. Ashour

  6. Physics Department, Faculty of Science, King Khalid University, P. O. Box 9004, Abha, 61413, Saudi Arabia

    Sayed Yousef

  7. Research Center for Advanced Materials Science (RCAMS), King Khalid University, P. O. Box 9004, Abha, 61413, Saudi Arabia

    Sayed Yousef

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Khamies Saber Shaaban, methodology, writing the manuscript, review the manuscript, and Badriah Mesfer Alotaibi, review the manuscript. Z.A. Alrowaili, reviews the manuscript M. S. Al-Buriahi, review the manuscript, A.Ashour, review the manuscript, and El Sayed Yousef, review the manuscript.

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Shaaban, K.S., Alotaibi, B.M., Alrowaili, Z.A. et al. Thermal and Mechanical Studies of Cerium Molybdenum Borosilicate Glasses and Glass–Ceramics. Silicon 15, 5233–5243 (2023). https://doi.org/10.1007/s12633-023-02433-3

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