Synthesis of l-ascorbate 6-phosphate☆

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Abstract

l-Ascorbate 6-phosphate (3) was prepared in aqueous medium at pH 8.5-9.0 by reaction of 6-bromo-6-deoxy-l-ascorbic acid with hydrogen phosphate ion at 25°. It was not detected by liquid chromatography in fresh spinach leaves, nor in mouse brain or lungs at a concentration above 30 μg/100 g of wet tissue.

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☆

Contribution No. 87-342J, from the Kansas State Agricultural Experiment Station, Manhattan, KS 66506, U.S.A.

1

Present address; College of medicine, University of Kansas, Kansas City, KS 66103, U.S.A.

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