Abstract
7-Bromo-5-phenyl-1,2-dihydro-3H-1,4-benztriazepin-2-one was obtained by thermolysis of the syn-4-phenylsemicarbazone of 2-aminobenzophenone. Its molecular and crystal structure were established by X-ray crystallography. The nature of the hydrogen bonds between molecules of the compound in solution and in the crystalline state was determined by IR spectroscopy and X-ray crystallography.
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Vlasiuk, S.V., Pavlovsky, V.I., Andronati, S.A. et al. 7-Bromo-5-phenyl-1,2-dihydro-3H-1,3,5-benztriazepin-2-one. Chemistry of Heterocyclic Compounds 36, 1077–1085 (2000). https://doi.org/10.1023/A:1002790116884
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DOI: https://doi.org/10.1023/A:1002790116884