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New 6-Arylsulfonyl-1,2-benzoisothiazol-3(2H)-one 1,1-Dioxides Derived from Diphenyl Sulfone Monosulfonyl Chlorides

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

Various methods were studied for the oxidation of 2-methyl-5-(phenylsulfonyl)benzenesulfamide and its derivatives. The oxidation by sodium dichromate in sulfuric acid was found most efficient. The effects of temperature, concentration, reagent ratio, and time of the oxidation reaction on the yield of the desired product were investigated. Conditions were proposed for obtaining the desired product in yields up to 95%. A synthesis was developed for a series of new saccharin derivatives.

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Authors and Affiliations

  1. Yaroslavl State Technical University, Yaroslavl, 150023, Russia

    A. V. Tarasov, P. O. Yablonsky & Yu. A. Moskvichev

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  1. A. V. Tarasov
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  2. P. O. Yablonsky
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  3. Yu. A. Moskvichev
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Tarasov, A.V., Yablonsky, P.O. & Moskvichev, Y.A. New 6-Arylsulfonyl-1,2-benzoisothiazol-3(2H)-one 1,1-Dioxides Derived from Diphenyl Sulfone Monosulfonyl Chlorides. Chemistry of Heterocyclic Compounds 39, 119–122 (2003). https://doi.org/10.1023/A:1023037228824

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