Consecutive catalytic hydroformylation-acetalization of unsaturated carbohydrates (glucals) to give the dimethyl acetal of 2-C-formyl-D-alditol derivatives using the catalytic system [Rh(µ-OMe)(cod)]2/P(O-o-ButC6H4)3/PPTS is strongly dependent on the protecting groups on the carbohydrate.
E. Fernández, A. Ruiz, C. Claver, S. Castillón and A. Polo, Chem. Commun., 1998, 1803 DOI: 10.1039/A804220I
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