SCHEDULED MAINTENANCE
Irradiation of eucarvone (I) adsorbed on silica gel or in trifluoroethanol gives, in addition to the two expected products (IIa and IIb), the bicyclo[4,1,0]enone (V), which subsequently undergoes[1,3]sigmatropic photorearrangement to dehydrocamphor (IV) and a cyclobutanone (VI).
T. Takino and H. Hart, J. Chem. Soc. D, 1970, 450 DOI: 10.1039/C29700000450
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