Reaction of formic acid with aqueous (NH4)6–[Mo7O24]yields the compound (NH4)3[(HCO)(Mo4O14)]·H2O which has been shown by X-ray crystallography to contain the discrete [(H2Mo8O28)]6– anion; this anion is related to the [H2Mo8O28]6– anion by replacement of its surface-bound protons with formyl groups.
R. D. Adams, W. G. Klemperer and R. Liu, J. Chem. Soc., Chem. Commun., 1979, 256 DOI: 10.1039/C39790000256
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