[Ni4(S2)(SCH2CH2S)4]2–, which can be obtained by reaction of NiCl2, Na2(SCH2CH2S), and Na2S2, is the first complex that contains polysulphide and thiolate ligands simultaneously; the related trinuclear thiolate [Ni3(SCH2CH2S)4]2– has a linear metal frame and is formed in the absence of Na2S2.
W. Tremel, B. Krebs and G. Henkel, J. Chem. Soc., Chem. Commun., 1986, 1527 DOI: 10.1039/C39860001527
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