Issue 22, 1994
From the journal:

Journal of the Chemical Society, Dalton Transactions

Synthesis and solution multinuclear magnetic resonance studies of homoleptic copper(I) complexes of sulfur, selenium and tellurium donor ligands

Jane R. Black  and  William Levason  

Abstract

The complexes [CuL4][O3SCF3](L = Me2S, Me2Se, Me2Te, Ph2S, Ph2Se or Ph2Te) and [Cu(L–L)2]PF6[L–L = RE(CH2)2ER (E = S or Se, R = Me or Ph); RE(CH2)3ER (E = S, Se or Te; R = Me or Ph)] have been prepared and characterised by analysis, IR, and in particular multinuclear NMR spectroscopy (1H, 77Se, 125Te and 63Cu). Variable-temperature NMR studies have been used to probe various exchange processes occurring in solution. For a limited number of complexes 63Cu NMR resonances have been observed, the first examples from Group 16 donor complexes.

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Article information

DOI
https://doi.org/10.1039/DT9940003225
Article type
Paper

J. Chem. Soc., Dalton Trans., 1994, 3225-3230

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Synthesis and solution multinuclear magnetic resonance studies of homoleptic copper(I) complexes of sulfur, selenium and tellurium donor ligands

J. R. Black and W. Levason, J. Chem. Soc., Dalton Trans., 1994, 3225 DOI: 10.1039/DT9940003225

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