SCHEDULED MAINTENANCE
The ester group in 3β-tosyloxy-5α-androstan-17-one has been replaced with several aliphatic and heterocyclic secondary amines, to give 3α-amines. Reductive amination of 5α-androstan-, 5β-androstan-, or androst-4-en-3-ones afforded mixtures of 3α- and 3β-amines, the proportions varying according to the conditions employed.
M. Davis, E. W. Parnell and J. Rosenbaum, J. Chem. Soc. C, 1966, 1983 DOI: 10.1039/J39660001983
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