Issue 0, 1982
From the journal:

Journal of the Chemical Society, Perkin Transactions 1

Conformational behaviour of medium-sized rings. Part 14. Tetra-anthranilides

Alireza Hoorfar,   W. David Ollis  and  J. Fraser Stoddart  

Abstract

The stepwise synthesis of N,N′,N″-trimethyltetra-anthranilide (13) is reported and the temperature dependence of the 1H n.m.r. spectrum of N-benzyl-N′,N″,N‴-trimethyltetra-anthranilide (15) is interpreted in terms of equilibration between three diastereoisomeric conformations in solution. Although there is 1H n.m.r. spectral evidence for the presence in solution at room temperature of at least six conformational diastereoisomers of (13), N,N′,N″,N‴-tetramethyltetra-anthranilide (14) appears to adopt a single conformation of high symmetry in solution.

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Article information

DOI
https://doi.org/10.1039/P19820001721
Article type
Paper

J. Chem. Soc., Perkin Trans. 1, 1982, 1721-1726

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Conformational behaviour of medium-sized rings. Part 14. Tetra-anthranilides

A. Hoorfar, W. D. Ollis and J. F. Stoddart, J. Chem. Soc., Perkin Trans. 1, 1982, 1721 DOI: 10.1039/P19820001721

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