The assignment of the structures (1)–(3) to janthitrems E-G, tremorgenic mycotoxins isolated from cultures of Penicillium janthinellum is based on a detailed study of their highfield 1H and 13C n.m.r. spectra. In the structure elucidation extensive use was made of heteronuclear 13C-{1H} selective population inversion (SPI) and homonuclear 1H-{1H} n.O.e. experiments.
A. E. de Jesus, P. S. Steyn, F. R. van Heerden and R. Vleggaar, J. Chem. Soc., Perkin Trans. 1, 1984, 697 DOI: 10.1039/P19840000697
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