Issue 21, 1989
From the journal:

Journal of the Chemical Society, Chemical Communications

Reaction of trialkylboranes with sodium diethyldihydroaluminate in the presence of 1,4-diazabicyclo[2.2.2]octane: a convenient, general method for preparation of sodium trialkylhydroborates

John L. Hubbard  

Abstract

Trialkylboranes in tetrahydrofuran solution, even those with exceptionally large steric requirements, react readily with toluene solutions of sodium diethyldihydroaluminate in the presece of 1,4-diazabicyclo[2.2.2]octane, resulting in a convenient and general preparation of sodium trialkylhydroborates.

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Article information

DOI
https://doi.org/10.1039/C39890001639
Article type
Paper

J. Chem. Soc., Chem. Commun., 1989, 1639-1640

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Reaction of trialkylboranes with sodium diethyldihydroaluminate in the presence of 1,4-diazabicyclo[2.2.2]octane: a convenient, general method for preparation of sodium trialkylhydroborates

J. L. Hubbard, J. Chem. Soc., Chem. Commun., 1989, 1639 DOI: 10.1039/C39890001639

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