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The structure of desertorin C, a metabolite of the mould Emericella desertorum, is confirmed as 4,4′,7,7′-tetramethoxy-5,5′-dimethyl-6,8′-bicoumarin (6), by its synthesis in racemic form. The key step involved the construction of the unsymmetrical biphenyl, 2,2′,4,6′-tetramethoxy-4′,6-dimethylbiphenyl (19), using dihydro-oxazole chemistry.
M. A. Rizzacasa and M. V. Sargent, J. Chem. Soc., Perkin Trans. 1, 1988, 2425 DOI: 10.1039/P19880002425
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