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Transmission Bragg edge spectroscopy measurements at ORNL Spallation Neutron Source

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Published under licence by IOP Publishing Ltd
, , Citation A S Tremsin et al 2010 J. Phys.: Conf. Ser. 251 012069 DOI 10.1088/1742-6596/251/1/012069

1742-6596/251/1/012069

Abstract

Results of neutron transmission Bragg edge spectroscopic experiments performed at the SNAP beamline of the Spallation Neutron Source are presented. A high resolution neutron counting detector with a neutron sensitive microchannel plate and Timepix ASIC readout is capable of energy resolved two dimensional mapping of neutron transmission with spatial accuracy of ∼55 μm, limited by the readout pixel size, and energy resolution limited by the duration of the initial neutron pulse. A two dimensional map of the Fe 110 Bragg edge position was obtained for a bent steel screw sample. Although the neutron pulse duration corresponded to ∼30 mÅ energy resolution for 15.3 m flight path, the accuracy of the Bragg edge position in our measurements was improved by analytical fitting to a few mÅ level. A two dimensional strain map was calculated from measured Bragg edge values with an accuracy of ∼few hundreds μistrain for 300s of data acquisition time.

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10.1088/1742-6596/251/1/012069