Skip to main content
SpringerLink
Log in

Determination of volatile organic compounds by solid-phase microextraction

  • Published:
Applied Biochemistry and Microbiology Aims and scope Submit manuscript

Abstract

The parameters of the process of isolation, concentration, and gas chromatographic analysis of volatile organic compounds by solid-phase microextraction were optimized. With different amounts of a mixture of essential oils, the conditions of reproducibility of their determination were established based on the absolute values of the squares of chromatographic peaks obtained by capillary gas chromatography. It was found that the efficiency of the extraction of volatile compounds from gas phase by sorption on mixed polymer (consisting of polydimethylsiloxane and divinylbenzene) was significantly influenced by the structure of their molecules, while the sorption time and their content in the liquid phase influenced the significance of determination.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Seurve, A.M., Diaz, M.A., and Voilley, A.J., J. Agric. Food Chem., 2000, vol. 48, no. 9, pp. 4296–4303.

    Article  Google Scholar 

  2. Misharina, T.A., Prikl. Analit. Khim., 2010, vol. 1, no. 2, pp. 12–19.

    Google Scholar 

  3. Kirchhoff, E. and Schieberle, P., J. Agric. Food Chem., 2001, vol. 49, no. 11, pp. 4304–4311.

    Article  CAS  PubMed  Google Scholar 

  4. Schieberle, P., Z. Lebensm. Unters. For, 1990, vol. 191, no. 1, pp. 206–209.

    Article  CAS  Google Scholar 

  5. Cho, I.H. and Peterson, D.G., Food Sci. Biotechnol., 2010, vol. 19, no. 3, pp. 575–582.

    Article  CAS  Google Scholar 

  6. Ettre, L.S., Headspace Analysis of Food and Flavours: Theory and Practice, Rouseff, R.L. and Cadwallader, K.R, Eds., New York: Acad. Plenum Publ., 2001.

  7. Meilgaard, M.C., Tech. Q. Master Brew. Assoc. Am., 1975, vol. 12, no. 1, pp. 151–168.

    CAS  Google Scholar 

  8. Golovnya, R.V. and Misharina, T.A., Zh. Anal. Khim., 1981, vol. 36, no. 7, pp. 1390–1398.

    CAS  Google Scholar 

  9. Arthur, C.L. and Pawliszyn, J., Anal. Chem., 1990, vol. 62, no. 7, pp. 2145–2148.

    Article  CAS  Google Scholar 

  10. Zhang, Z. and Pawliszyn, J., Anal. Chem., 1993, vol. 65, no. 5, pp. 1843–1852.

    Article  CAS  Google Scholar 

  11. Nongonierma, A., Cayot, P., Le Quere, J.L., Springett, M., and Voilley, A.J., Food Rew. Int., 2006, vol. 22, no. 1, pp. 51–94.

    Article  CAS  Google Scholar 

  12. Scarlata, C.J. and Ebeker, S.E., J. Agric. Food Chem., 1999, vol. 47, no. 15, pp. 2505–2508.

    Article  CAS  PubMed  Google Scholar 

  13. Vas, G.Y., Koteleky, K., Farkas, M., Dobo, A., and Vekey, K., Am. J. Enol. Vitc., 1998, vol. 49, no. 1, pp. 100–104.

    CAS  Google Scholar 

  14. Rocha, S., Ramarheira, V., Barros, A., Delgadillo, I., and Coimbra, M.A., J. Agric. Food Chem., 2001, vol. 49, no. 26, pp. 5142–5151.

    Article  CAS  PubMed  Google Scholar 

  15. Bicchi, C.P., Panero, O.M., Pellegrino, G.M., and Vanni, A.C., J. Agric. Food Chem., 1997, vol. 45, no. 24, pp. 4680–4686.

    Article  CAS  Google Scholar 

  16. Zhu, J.Y. and Chai, X.-C., Curr. Anal. Chem., 2005, vol. 1, no. 1, pp. 79–83.

    Article  CAS  Google Scholar 

  17. Ruiz, J.A., Quilez, J., Mestres, M., and Guasch, L., Cereal Chem., 2003, vol. 80, no. 1, pp. 255–259.

    Article  CAS  Google Scholar 

  18. Jang, D.-M. and Ebeler, S.E., J. Agric. Food Chem., 2003, vol. 51, no. 1, pp. 200–205.

    Article  Google Scholar 

  19. Fabre, M., Aubry, V., and Guichard, E., J. Agric. Food Chem., 2002, vol. 50, no. 8, pp. 1497–1501.

    Article  CAS  PubMed  Google Scholar 

  20. Joeunne, E. and Crouzet, J., J. Agric. Food Chem., 2000, vol. 48, no. 7, pp. 1273–1277.

    Article  Google Scholar 

  21. Cavalli, J.F., Fernandez, X., Lizzani-Cuvelier, L., and Loiseau, A.M., J. Agric. Food Chem., 2003, vol. 51, no. 21, pp. 7709–7713.

    Article  CAS  PubMed  Google Scholar 

  22. Kanavouras, A., Kiritsakis, A., and Hernandez, R.J., Food Chem., 2005, vol. 90, no. 1, pp. 69–76.

    Article  CAS  Google Scholar 

  23. Vichi, S., Castellote, A.I., Pizzale, L., Conte, L.S., Buxaderas, S., and Lopez-Tamames, E., J. Chromatogr., A, 2003, vol. 983, no. 1, pp. 19–27.

    Article  CAS  Google Scholar 

  24. Vergnais, L., Masson, F., Montel, M.C., Berdague, J.L., and Talon, R., J. Agric. Food Chem., 1998, vol. 46, no. 1, pp. 228–234.

    Article  CAS  PubMed  Google Scholar 

  25. Misharina, T.A., Appl. Biochem. Microbiol., 2002, vol. 38, no. 5, pp. 480–486.

    Article  CAS  Google Scholar 

  26. Misharina, T.A., Appl. Biochem. Microbiol., 2004, vol. 40, no. 1, pp. 104–107.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Emanuel Institute of Biochemical Physics, Russian Academy of Sciences, Moscow, 119334, Russia

    T. A. Misharina, M. B. Terenina & N. I. Krikunova

  2. Plekhanov Russian University of Economics, Moscow, 117997, Russia

    T. A. Misharina

Authors
  1. T. A. Misharina
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. M. B. Terenina
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. N. I. Krikunova
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to T. A. Misharina.

Additional information

Original Russian Text © T.A. Misharina, M.B. Terenina, N.I. Krikunova, 2017, published in Prikladnaya Biokhimiya i Mikrobiologiya, 2017, Vol. 53, No. 5, pp. 534–543.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Misharina, T.A., Terenina, M.B. & Krikunova, N.I. Determination of volatile organic compounds by solid-phase microextraction. Appl Biochem Microbiol 53, 600–609 (2017). https://doi.org/10.1134/S000368381705012X

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S000368381705012X

Keywords

Search

Navigation