Abstract
Comparison of various laboratory procedures for the synthesis of palladium acetate demonstrated that the purest product containing no nitrite or nitrate impurities is formed in up to 90% yields upon the reaction of palladium nitrate with alkali metal acetates in aqueous acetic acid. Other laboratory syntheses are more labor-consuming and do not ensure high purity of the product. The synthesis by-products are described and possible reaction schemes are proposed.
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Original Russian Text © I.P. Stolyarov, L.I. Demina, N.V. Cherkashina, 2011, published in Zhurnal Neorganicheskoi Khimii, 2011, Vol. 56, No. 10, pp. 1611–1616.
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Stolyarov, I.P., Demina, L.I. & Cherkashina, N.V. Preparative synthesis of palladium(II) acetate: Reactions, intermediates, and by-products. Russ. J. Inorg. Chem. 56, 1532–1537 (2011). https://doi.org/10.1134/S003602361110024X
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DOI: https://doi.org/10.1134/S003602361110024X