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＜departmental bulletin paper＞
Role of Microwave Irradiation for the Preparation of Nickel Nanoparticles by a Polyol Method

Creator
Author PID
K001853
Creator Name
Tsuji, Masaharu
辻, 正治
ツジ, マサハル
Affiliation
Affiliation Name
Institute for Materials Chemistry and Engineering, Kyushu University | CREST, JST
九州大学先導物質科学研究所 | 戦略的創造研究推進機構
Creator Name
Hashimoto, Masayuki
橋本, 昌幸
ハシモト, マサユキ
Affiliation
Affiliation Name
Department of Applied Science for Electronics and Materials, Interdisciplinary Graduate School of Engineering Sciences, Kyushu University
九州大学大学院総合理工学研究科量子プロセス理工学専攻
Creator Name
Nishizawa, Yuki
西澤, 幸
ニシザワ, ユキ
Affiliation
Affiliation Name
Department of Applied Science for Electronics and Materials, Interdisciplinary Graduate School of Engineering Sciences, Kyushu University
九州大学大学院総合理工学研究科量子プロセス理工学専攻
Author PID
K001872
Creator Name
Tsuji, Takeshi
辻, 剛志
ツジ, タケシ
Affiliation
Affiliation Name
CREST, JST | Institute for Materials Chemistry and Engineering, Kyushu University
九州大学先導物質科学研究所
Language
English
Publisher
九州大学大学院総合理工学府
Interdisciplinary Graduate School of Engineering Sciences, Kyushu University
Date
2004-09
Source Title
Engineering sciences reports, Kyushu University
Vol
26
Issue
2
First Page
205
Last Page
208
Publication Type
Version of Record
Access Rights
open access
JaLC DOI
https://doi.org/10.15017/16726
Related DOI
九州大学大学院総合理工学報告 || 26(2) || p205-208
Engineering sciences reports, Kyushu University || 26(2) || p205-208
http://www.tj.kyushu-u.ac.jp/
http://www.tj.kyushu-u.ac.jp/info/online/
Related URI
九州大学大学院総合理工学報告 || 26(2) || p205-208
Engineering sciences reports, Kyushu University || 26(2) || p205-208
http://www.tj.kyushu-u.ac.jp/
http://www.tj.kyushu-u.ac.jp/info/online/
Relation
九州大学大学院総合理工学報告 || 26(2) || p205-208
Engineering sciences reports, Kyushu University || 26(2) || p205-208
http://www.tj.kyushu-u.ac.jp/
http://www.tj.kyushu-u.ac.jp/info/online/
Abstract Ni(OH)2 was reduced by ethylene glycol, in the presence of polyvinylpyrrolidone (PVP) under microwave (MW) heating in a pulse mode and oil-bath heating. The temperature profile in the two heating meth...ods was controlled to be identical in order to determine whether the role of MW irradiation for the preparation of nickel nanoparticles is only thermal or not. Aggregated spherical nickel nanoparticles with diameters of 52 nm were produced under MW heating for 35 min, while larger monodispersed spherical nanoparticles with diameters of 204 nm were prepared in oil-bath heating for 35 min. Different size and dispersion pattern of nanoparticles under the two heating methods indicated that MW irradiation affects the nucleation, growth, and aggregation of Ni nanoparticles.show more

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Details

Record ID
16726
Peer-Reviewed
Refereed
Subject Terms
Metals and alloys
Nanomaterials
Microwave heating
Polyol method
Electron microscopy
ISSN
1346-7883
NCID
AA1147319X
Created Date 2010.03.09
Modified Date 2020.11.17

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