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Licensed Unlicensed Requires Authentication Published by De Gruyter May 22, 2014

Structural changes in spruce wood during different steps of steam explosion pretreatment

  • Muhammad Muzamal , Kerstin Jedvert , Hans Theliander and Anders Rasmuson EMAIL logo
From the journal Holzforschung

Abstract

Steam explosion (SE) is a promising hydrothermal pretreatment technology for future biorefineries. In this study, the three steps of the steam explosion process, (1) the steam treatment (2) the explosion, and (3) the impact step were separately considered and their effects on structural changes of wood were studied. The SE experiments were performed on single wood pieces in different experimental set-ups at 7 and 14 bar pressure with 5 and 10 min treatment times. Mercury porosimetry and environmental scanning electron microscopy analyses were conducted to characterise both internal and external changes in the wood. It was found that the explosion step is not responsible for the disintegration of the wood material into small pieces; instead, the disintegration occurs due to impact of softened wood chips. However, the porosity profiles of the tracheids change during the explosion step. Altogether, all three steps of the SE process contribute in a synergistic way to an increase in pore size and total intrusion volume.


Corresponding author: Anders Rasmuson, Chemical and Biological Engineering, Chalmers University of Technology, Gothenburg, Sweden; and Wallenberg Wood Science Center, Department of Fibre and Polymer Technology, KTH Royal Institute of Technology, Stockholm, Sweden, e-mail:

Acknowledgements

Chalmers Energy Initiative and Wallenberg Wood Science Center are gratefully acknowledged for financial support.

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Received: 2013-12-7
Accepted: 2014-4-24
Published Online: 2014-5-22
Published in Print: 2015-1-1

©2015 by De Gruyter

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