Notizen: Cyclophanes, XXXIV [1]: Preparation and X-Ray Structure of [2.2](5,6)Indanocyclophane

Peter G. Jones; Graham Bodwell; Henning Hopf

doi:10.1515/znb-1990-0818

Open Access Published by De Gruyter June 2, 2014

Notizen: Cyclophanes, XXXIV [1]

Preparation and X-Ray Structure of [2.2](5,6)Indanocyclophane

Peter G. Jones , Graham Bodwell and Henning Hopf

From the journal Zeitschrift für Naturforschung B

https://doi.org/10.1515/znb-1990-0818

The title compound 3 was prepared by pyrolysis of the corresponding bis-sulfone 2 and subjected to X-ray structural analysis; space group P 1̅, a = 477.0(1), b = 625.6(2), c = 1363.6(3) pm, α = 82.79(2), β = 83.43(2), γ = 78.18(3)°, Ζ = 1, R = 0.058 for 900 reflections. The molecule contains a crystallographic symmetry centre, thus confirming the anti configuration.

Received: 1990-2-20

Published Online: 2014-6-2

Published in Print: 1990-8-1

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Notizen: Cyclophanes, XXXIV [1]

Preparation and X-Ray Structure of [2.2](5,6)Indanocyclophane

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