Abstract
Submicrometer-grained (SMG) microstructures are produced in an Al–Mg–Si alloy (6061) by subjecting peak-aged and overaged billets of the alloy to intense plastic strain by a process known as equal channel angular extrusion. Two types of refined structure are distinguished by optical and transmission electron microscopy. One structure is created through intense deformation (four extrusion passes through a 90° die, ∈ = 4.62) by dynamic rotational recrystallization and is a well-formed grain (fragmented) structure with a mean fragment or grain size of 0.2–0.4 µm. The other structure is produced by post-extrusion annealing through static migration recrystallization, resulting in a grain size of 5–15 µm. Intense deformation of peak-aged material to a true strain ∈ of 4.62 (four passes) produces a strong, ductile, uniform, fine, and high angle grain boundary microstructure with increased stability against static recrystallization as compared to the overaged material.
Similar content being viewed by others
References
R. Z. Valiev, A. V. Kornikov, and R. R. Mulyokov, Mater. Sci. Eng. A168, 141 (1993).
I. Saunders and J. Nutting, Metall. Sci. 18, 571 (1984).
H. J. Zughaer and J. Nutting, Mater. Sci. Technol. 8, 1104 (1992).
J. A. Wert and L. K. Austin, Metall. Trans. A19, 617 (1988).
J. A. Wert, N. E. Paton, C. H. Hamilton, and M. W. Mahoney, Metall. Trans. A12, 1267 (1981).
J. Pilling and N. Ridley, Superplasticity in Crystalline Solids (The Institute of Metals, London, 1989).
V. M. Segal, Invention Certificate of the USSR, No. 575892, 1977.
V. M. Segal, V. I. Reznikov, A. E. Drobyshevkiy, and V. I. Kopylov, Russian Metall. (English Translation), 1, 99 (1981).
V. M. Segal, Proc. 5th Int. Aluminum Extrusion Technology Seminar (1992), Vol. 2, p. 403.
V. M. Segal, Proceedings of the First International Conference on Processing Material for Properties (TMS, Warrendale, PA, 1993), p. 947.
B. Bay, N. Hansen, D. A. Hughes, and D. Kulmann-Wilsdorf, Acta Metall. Mater. 40 (3), 205 (1992).
M. T. Lyttle and J. A. Wert, J. Mater. Sci. 29, 3342 (1994).
H. Gudmunsson, D. Brooks, and J. A. Wert, Acta Metall. 39, 19 (1991).
V. M. Segal, R. E. Goforth, and K. T. Hartwig, United States Patent No. 5400 633, Mar. 28, 1995.
V. M. Segal, R. E. Goforth, and K. T. Hartwig, Proceedings of the First International Conference on Processing Materials for Properties (TMS, Warrendale, PA, 1993), p. 971.
S. Ferrasse, “Grain Refinement Using Equal Channel Angular Extrusion In Bulk Sections of Copper 101 and Aluminum Alloys 3003 and 6061,” Masters Thesis, Texas A&M University, May 1995.
R. E. Goforth, V. M. Segal, K. T. Hartwig, and S. Ferrasse, Superplasticity and Superplastic Forming, edited by A. Ghosh and T. Bieler (TMS, Warrendale, PA, 1995), p. 25.
M. A. Zaidi and J. A. Wert, Treatise on Mat. Sci. and Tech. 31, 137 (1989).
E. Nes, Acta Metall. 24, 391 (1976).
E. Hornbogen, Fundamental Aspects of Structural Alloy Design (Plenum Press, New York, 1977).
R. Sandstrom, Z. Metallk. 11, 741 (1980).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Ferrasse, S., Segal, V.M., Hartwig, K.T. et al. Development of a submicrometer-grained microstructure in aluminum 6061 using equal channel angular extrusion. Journal of Materials Research 12, 1253–1261 (1997). https://doi.org/10.1557/JMR.1997.0173
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1557/JMR.1997.0173